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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-31395-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-80892 Preparation: 5030B <br /> MS Lab Sample ID: 720-31497-A-3 MS Analysis Batch: 720-80892 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 110110014.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 11/01/2010 1617 Final Weight/Volume: 10 mL <br /> Date Prepared: 11/01/2010 1617 <br /> MSD Lab Sample ID: 720-31497-A-3 MSD Analysis Batch: 720-80892 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 110110015.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 11/01/2010 1649 Final Weight/Volume: 10 mL <br /> Date Prepared: 11/01/2010 1649 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 94 96 60-140 2 20 <br /> 1,1-Dichloroethane 104 102 60-140 2 20 <br /> Dichlorodifluoromethane 87 81 38-140 6 20 <br /> Vinyl chloride 95 91 58-140 4 20 <br /> Chloroethane 97 95 51 -140 2 20 <br /> Trichlorofluoromethane 109 102 60-140 6 20 <br /> Methylene Chloride 96 96 40-140 0 20 <br /> trans-1,2-Dichloroethene 88 89 60-140 1 20 <br /> cis-1,2-Dichloroethene 120 118 60-140 2 20 <br /> Chloroform 110 105 60-140 4 20 <br /> 1,1,1-Trichloroethane 110 104 60-140 6 20 <br /> Carbon tetrachloride 111 104 60-140 6 20 <br /> 1,2-Dichloroethane 116 110 60-140 6 20 <br /> Trichloroethene 104 102 60-140 1 20 <br /> 1,2-Dichloropropane 106 105 60-140 1 20 <br /> Dichlorobromomethane 116 112 60-140 4 20 <br /> trans-1,3-Dichloropropene 121 114 60-140 5 20 <br /> cis-1,3-Dichloropropene 115 112 60-140 3 20 <br /> 1,1,2-Trichloroethane 116 112 60-140 3 20 <br /> Tetrachloroethene 110 105 60-140 4 20 <br /> Chlorodibromomethane 119 113 60-140 5 20 <br /> Chlorobenzene 103 101 60-140 2 20 <br /> Bromoform 104 100 56-140 4 20 <br /> 1,1,2,2-Tetrachloroethane 104 104 60-140 0 20 <br /> 1,3-Dichlorobenzene 107 108 60-140 0 20 <br /> 1,4-Dichlorobenzene 106 105 60-140 1 20 <br /> 1,2-Dichlorobenzene 110 108 60-140 2 20 <br /> Chloromethane 98 95 52-140 4 20 <br /> Bromomethane 91 90 23-140 1 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 94 92 60-140 2 20 <br /> TestAmerica San Francisco Page 82 of 88 <br />