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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-31617-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-81384 Preparation: 5030B <br /> MS Lab Sample ID: 720-31617-1 Analysis Batch: 720-81384 Instrument ID: HP4 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 110810027.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 11/08/2010 2230 Final Weight/Volume: 10 mL <br /> Date Prepared: 11/08/2010 2230 <br /> MSD Lab Sample ID: 720-31617-1 Analysis Batch: 720-81384 Instrument ID: HP4 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 110810028.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 11/08/2010 2302 Final Weight/Volume: 10 mL <br /> Date Prepared: 11/08/2010 2302 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 104 106 60-140 2 20 <br /> 1,1-Dichloroethane 109 111 60-140 2 20 <br /> Dichlorodifluoromethane 106 105 38-140 1 20 <br /> Vinyl chloride 104 102 58-140 2 20 <br /> Chloroethane 107 105 51 -140 2 20 <br /> Trichlorofluoromethane 110 110 60-140 0 20 <br /> Methylene Chloride 98 101 40-140 3 20 <br /> trans-1,2-Dichloroethene 92 96 60-140 4 20 <br /> cis-1,2-Dichloroethene 120 122 60-140 2 20 <br /> Chloroform 111 114 60-140 3 20 <br /> 1,1,1-Trichloroethane 105 111 60-140 5 20 <br /> Carbon tetrachloride 106 113 60-140 6 20 <br /> 1,2-Dichloroethane 107 112 60-140 4 20 <br /> Trichloroethene 100 104 60-140 3 20 <br /> 1,2-Dichloropropane 105 108 60-140 3 20 <br /> Dichlorobromomethane 117 121 60-140 3 20 <br /> trans-1,3-Dichloropropene 119 125 60-140 5 20 <br /> cis-1,3-Dichloropropene 113 117 60-140 4 20 <br /> 1,1,2-Trichloroethane 108 114 60-140 5 20 <br /> Tetrachloroethene 99 104 60-140 5 20 <br /> Chlorodibromomethane 110 115 60-140 4 20 <br /> Chlorobenzene 102 105 60-140 3 20 <br /> Bromoform 104 113 56-140 8 20 <br /> 1,1,2,2-Tetrachloroethane 108 116 60-140 8 20 <br /> 1,3-Dichlorobenzene 104 107 60-140 3 20 <br /> 1,4-Dichlorobenzene 102 106 60-140 4 20 <br /> 1,2-Dichlorobenzene 102 106 60-140 3 20 <br /> Chloromethane 111 112 52-140 1 20 <br /> Bromomethane 100 104 23-140 4 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 96 102 60-140 6 20 <br /> TestAmerica San Francisco Page 27 of 36 <br />