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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-32093-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-82789 Preparation: 5030B <br /> MS Lab Sample ID: 720-32103-B-21 MS Analysis Batch: 720-82789 Instrument ID: HP4 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 120710012.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 12/07/2010 1438 Final Weight/Volume: 10 mL <br /> Date Prepared: 12/07/2010 1438 <br /> MSD Lab Sample ID: 720-32103-B-21 MSD Analysis Batch: 720-82789 Instrument ID: HP4 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 120710013.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 12/07/2010 1510 Final Weight/Volume: 10 mL <br /> Date Prepared: 12/07/2010 1510 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 89 92 60-140 3 20 <br /> 1,1-Dichloroethane 97 99 60-140 2 20 <br /> Dichlorodifluoromethane 69 71 38-140 2 20 <br /> Vinyl chloride 92 90 58-140 2 20 <br /> Chloroethane 107 105 51 -140 2 20 <br /> Trichlorofluoromethane 93 95 60-140 2 20 <br /> Methylene Chloride 91 92 40-140 1 20 <br /> trans-1,2-Dichloroethene 83 85 60-140 2 20 <br /> cis-1,2-Dichloroethene 96 102 60-140 1 20 <br /> Chloroform 94 97 60-140 2 20 <br /> 1,1,1-Trichloroethane 102 104 60-140 1 20 <br /> Carbon tetrachloride 109 112 60-140 3 20 <br /> 1,2-Dichloroethane 97 98 60-140 1 20 <br /> Trichloroethene 96 97 60-140 1 20 <br /> 1,2-Dichloropropane 101 102 60-140 1 20 <br /> Dichlorobromomethane 100 104 60-140 4 20 <br /> trans-1,3-Dichloropropene 115 117 60-140 1 20 <br /> cis-1,3-Dichloropropene 110 112 60-140 2 20 <br /> 1,1,2-Trichloroethane 104 105 60-140 1 20 <br /> Tetrachloroethene 96 96 60-140 1 20 <br /> Chlorodibromomethane 109 110 60-140 0 20 <br /> Chlorobenzene 96 99 60-140 2 20 <br /> Bromoform 102 104 56-140 2 20 <br /> 1,1,2,2-Tetrachloroethane 114 112 60-140 2 20 <br /> 1,3-Dichlorobenzene 104 104 60-140 0 20 <br /> 1,4-Dichlorobenzene 101 102 60-140 1 20 <br /> 1,2-Dichlorobenzene 102 104 60-140 2 20 <br /> Chloromethane 98 97 52-140 1 20 <br /> Bromomethane 107 103 23-140 3 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 96 100 60-140 5 20 <br /> TestAmerica San Francisco Page 22 of 35 <br />