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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-32093-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-82791 Preparation: 5030B <br /> MS Lab Sample ID: 720-32120-A-1 MS Analysis Batch: 720-82791 Instrument ID: HP9 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 12071012.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 12/07/2010 1435 Final Weight/Volume: 10 mL <br /> Date Prepared: 12/07/2010 1435 <br /> MSD Lab Sample ID: 720-32120-A-1 MSD Analysis Batch: 720-82791 Instrument ID: HP9 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 12071013.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 12/07/2010 1507 Final Weight/Volume: 10 mL <br /> Date Prepared: 12/07/2010 1507 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 106 103 60-140 2 20 <br /> 1,1-Dichloroethane 99 98 60-140 1 20 <br /> Dichlorodifluoromethane 88 84 38-140 5 20 <br /> Vinyl chloride 92 91 58-140 1 20 <br /> Chloroethane 106 105 51 -140 1 20 <br /> Trichlorofluoromethane 120 113 60-140 6 20 <br /> Methylene Chloride 92 92 40-140 1 20 <br /> trans-1,2-Dichloroethene 95 94 60-140 1 20 <br /> cis-1,2-Dichloroethene 112 110 60-140 2 20 <br /> Chloroform 99 98 60-140 1 20 <br /> 1,1,1-Trichloroethane 113 112 60-140 1 20 <br /> Carbon tetrachloride 113 112 60-140 1 20 <br /> 1,2-Dichloroethane 91 90 60-140 1 20 <br /> Trichloroethene 103 103 60-140 1 20 <br /> 1,2-Dichloropropane 93 91 60-140 1 20 <br /> Dichlorobromomethane 98 98 60-140 0 20 <br /> trans-1,3-Dichloropropene 95 95 60-140 0 20 <br /> cis-1,3-Dichloropropene 94 94 60-140 0 20 <br /> 1,1,2-Trichloroethane 92 92 60-140 1 20 <br /> Tetrachloroethene 105 103 60-140 2 20 <br /> Chlorodibromomethane 91 91 60-140 0 20 <br /> Chlorobenzene 101 100 60-140 0 20 <br /> Bromoform 102 103 56-140 0 20 <br /> 1,1,2,2-Tetrachloroethane 108 108 60-140 0 20 <br /> 1,3-Dichlorobenzene 105 104 60-140 2 20 <br /> 1,4-Dichlorobenzene 102 100 60-140 2 20 <br /> 1,2-Dichlorobenzene 99 99 60-140 0 20 <br /> Chloromethane 92 89 52-140 3 20 <br /> Bromomethane 100 98 23-140 2 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 112 110 60-140 2 20 <br /> TestAmerica San Francisco Page 27 of 35 <br />