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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-30985-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-79691 Preparation: 5030B <br /> MS Lab Sample ID: 720-30969-B-3 MS Analysis Batch: 720-79691 Instrument ID: CHMSV2 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 10121011.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/12/2010 1336 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/12/2010 1336 <br /> MSD Lab Sample ID: 720-30969-B-3 MSD Analysis Batch: 720-79691 Instrument ID: CHMSV2 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 10121012.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/12/2010 1408 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/12/2010 1408 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 98 99 60-140 1 20 <br /> 1,1-Dichloroethane 101 103 60-140 2 20 <br /> Dichlorodifluoromethane 86 86 38-140 0 20 <br /> Vinyl chloride 89 89 58-140 0 20 <br /> Chloroethane 104 105 51 -140 1 20 <br /> Trichlorofluoromethane 115 120 60-140 4 20 <br /> Methylene Chloride 98 101 40-140 3 20 <br /> trans-1,2-Dichloroethene 97 100 60-140 2 20 <br /> cis-1,2-Dichloroethene 75 74 60-140 0 20 4 4 <br /> Chloroform 102 105 60-140 2 20 <br /> 1,1,1-Trichloroethane 108 110 60-140 2 20 <br /> Carbon tetrachloride 106 108 60-140 1 20 <br /> 1,2-Dichloroethane 106 108 60-140 1 20 <br /> Trichloroethene 87 86 60-140 0 20 <br /> 1,2-Dichloropropane 100 103 60-140 3 20 <br /> Dichlorobromomethane 112 114 60-140 2 20 <br /> trans-1,3-Dichloropropene 105 107 60-140 2 20 <br /> cis-1,3-Dichloropropene 101 104 60-140 3 20 <br /> 1,1,2-Trichloroethane 100 103 60-140 3 20 <br /> Tetrachloroethene 100 101 60-140 1 20 <br /> Chlorodibromomethane 111 113 60-140 2 20 <br /> Chlorobenzene 94 97 60-140 3 20 <br /> Bromoform 100 103 56-140 3 20 <br /> 1,1,2,2-Tetrachloroethane 105 108 60-140 3 20 <br /> 1,3-Dichlorobenzene 100 102 60-140 2 20 <br /> 1,4-Dichlorobenzene 96 98 60-140 2 20 <br /> 1,2-Dichlorobenzene 97 99 60-140 2 20 <br /> Chloromethane 94 94 52-140 1 20 <br /> Bromomethane 89 93 23-140 3 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 103 103 60-140 1 20 <br /> TestAmerica San Francisco Page 20 of 23 <br />