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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-32465-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-84089 Preparation: 5030B <br /> MS Lab Sample ID: 720-32474-A-4 MS Analysis Batch: 720-84089 Instrument ID: HP4 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 123010020.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 12/30/2010 1636 Final Weight/Volume: 10 mL <br /> Date Prepared: 12/30/2010 1636 <br /> MSD Lab Sample ID: 720-32474-A-4 MSD Analysis Batch: 720-84089 Instrument ID: HP4 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 123010021.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 12/30/2010 1708 Final Weight/Volume: 10 mL <br /> Date Prepared: 12/30/2010 1708 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 90 91 60-140 2 20 <br /> 1,1-Dichloroethane 98 100 60-140 2 20 <br /> Dichlorodifluoromethane 66 67 38-140 1 20 <br /> Vinyl chloride 84 91 58-140 8 20 <br /> Chloroethane 90 96 51 -140 7 20 <br /> Trichlorofluoromethane 93 94 60-140 1 20 <br /> Methylene Chloride 97 99 40-140 1 20 <br /> trans-1,2-Dichloroethene 84 89 60-140 5 20 <br /> cis-1,2-Dichloroethene 117 116 60-140 1 20 <br /> Chloroform 101 101 60-140 0 20 <br /> 1,1,1-Trichloroethane 95 94 60-140 2 20 <br /> Carbon tetrachloride 96 92 60-140 3 20 <br /> 1,2-Dichloroethane 100 100 60-140 0 20 <br /> Trichloroethene 102 100 60-140 2 20 <br /> 1,2-Dichloropropane 104 104 60-140 0 20 <br /> Dichlorobromomethane 110 108 60-140 2 20 <br /> trans-1,3-Dichloropropene 115 113 60-140 2 20 <br /> cis-1,3-Dichloropropene 111 112 60-140 1 20 <br /> 1,1,2-Trichloroethane 110 109 60-140 2 20 <br /> Tetrachloroethene 98 92 60-140 6 20 <br /> Chlorodibromomethane 110 109 60-140 1 20 <br /> Chlorobenzene 102 101 60-140 1 20 <br /> Bromoform 110 111 56-140 0 20 <br /> 1,1,2,2-Tetrachloroethane 110 112 60-140 2 20 <br /> 1,3-Dichlorobenzene 104 101 60-140 3 20 <br /> 1,4-Dichlorobenzene 97 94 60-140 3 20 <br /> 1,2-Dichlorobenzene 104 102 60-140 2 20 <br /> Chloromethane 83 95 52-140 14 20 <br /> Bromomethane 93 99 23-140 6 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 92 90 60-140 2 20 <br /> TestAmerica San Francisco Page 28 of 32 <br />