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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-32186-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-83106 Preparation: 5030B <br /> MS Lab Sample ID: 720-32199-A-10 MS Analysis Batch: 720-83106 Instrument ID: HP12 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 12101032.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 12/10/2010 2330 Final Weight/Volume: 10 mL <br /> Date Prepared: 12/10/2010 2330 <br /> MSD Lab Sample ID: 720-32199-A-10 MSD Analysis Batch: 720-83106 Instrument ID: HP12 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 12101033.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 12/10/2010 2359 Final Weight/Volume: 10 mL <br /> Date Prepared: 12/10/2010 2359 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 87 82 60-140 6 20 <br /> 1,1-Dichloroethane 103 99 60-140 3 20 <br /> Dichlorodifluoromethane 109 111 38-140 2 20 <br /> Vinyl chloride 65 70 58-140 2 20 <br /> Chloroethane 112 113 51 -140 1 20 <br /> Trichlorofluoromethane 106 107 60-140 1 20 <br /> Methylene Chloride 95 92 40-140 3 20 <br /> trans-1,2-Dichloroethene 81 78 60-140 3 20 <br /> cis-1,2-Dichloroethene 115 110 60-140 3 20 <br /> Chloroform 110 107 60-140 2 20 <br /> 1,1,1-Trichloroethane 101 97 60-140 4 20 <br /> Carbon tetrachloride 98 95 60-140 4 20 <br /> 1,2-Dichloroethane 106 106 60-140 0 20 <br /> Trichloroethene 89 89 60-140 0 20 <br /> 1,2-Dichloropropane 105 104 60-140 0 20 <br /> Dichlorobromomethane 113 115 60-140 1 20 <br /> trans-1,3-Dichloropropene 111 112 60-140 1 20 <br /> cis-1,3-Dichloropropene 108 109 60-140 0 20 <br /> 1,1,2-Trichloroethane 111 111 60-140 1 20 <br /> Tetrachloroethene 87 86 60-140 1 20 <br /> Chlorodibromomethane 109 109 60-140 1 20 <br /> Chlorobenzene 101 100 60-140 1 20 <br /> Bromoform 109 107 56-140 2 20 <br /> 1,1,2,2-Tetrachloroethane 121 120 60-140 1 20 <br /> 1,3-Dichlorobenzene 100 99 60-140 0 20 <br /> 1,4-Dichlorobenzene 101 100 60-140 0 20 <br /> 1,2-Dichlorobenzene 98 99 60-140 1 20 <br /> Chloromethane 104 109 52-140 5 20 <br /> Bromomethane 103 102 23-140 0 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 85 83 60-140 2 20 <br /> TestAmerica San Francisco Page 22 of 25 <br />