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MATRIX SPIKE SAMPLE DATA REPORT <br /> TOTAL Metals <br /> Client Lot #. . . . A0I290433 Matrix. . . . . . . . . . WATER <br /> Date Sampled. . . : 09/16/10 10:40 Date Received. . : 09/17/10 <br /> SAMPLE SPIKE MEASRD PERCNT PREPARATION— WORK <br /> PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE ORDER # <br /> MS Lot—Sample #: COI170487-003 Prep Batch #. . . : 0277203 <br /> Mercury <br /> 93.0 5.0 118 ng/L CFR136A 1631E 10/04-10/05/10 L64991E0 <br /> Qualifiers: NC,MSB <br /> 93.0 5.0 88.8 ng/L CFR136A 1631E 10/04-10/05/10 L64991E1 <br /> Qualifiers: NC,MSB <br /> Dilution Factor: 10 <br /> Analysis Time. . : 11:01 Instrument ID. . : H3 Analyst ID. . . . . : 002260 <br /> NOTE(S) <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> NC The recovery andlor RPD were not calculated. <br /> MSB The recovery and RPD may be outside control limits because the sample amount was greater than 4X the spike amount. <br /> North Canton Page 36 of 137 25 <br />