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METALS PREPARATION SUMMARY <br /> Preparation Type Matrix Amount of Standard added to LCS&MS/MSD Initial Sample Vol/Wt Final Sample <br /> Volume <br /> Amount Standard name <br /> ICP water 1 mL Ag 50 mL 50 mL <br /> 1 mL ICP-1 <br /> 1.0 mL ICP-2A <br /> ICPMS water 0.5ml ICPMS-1 50 mL 50 mL <br /> 0.5ml ICPMS-2 <br /> Hg-CVAA water 5 mL(LCS) HG-1 100 mL 100 mL <br /> 1 mL(MS/MSD) HG-1 <br /> Hg-CVAF(low level) water D.2 mL(LCS/MS/MSD) HG ICAL 40 ml 40 ml <br /> ICP solid 2 mL Ag 1.00+/-.02g 100 mL <br /> 2 mL ICP-1 <br /> 2 mL ICP-2A <br /> ICPMS solid 1ml ICPMS-1 1.00+/-.02g 100ml <br /> 1ml ICPMS-2 <br /> Hg-CVAA solid 5 mL(LCS) HG-1 0.60+/-.01g 100 mL <br /> 1 mL(MS/MSD) HG-1 <br /> ICP TCLP 1 mL(LCS) Ag 50 mL 50 mL <br /> 1 mL(LCS) ICP-1 <br /> ICP TCLP 0.5 mL(MS/MSD) TCLP Spike I RCRA 50 mL 50 mL <br /> ICP TCLP 1 mL(MS/MSD) TCLP Spike 11 Non-RCRA 50 mL 50 mL <br /> Hg-CVAA TCLP 5 mL(LCS) HG-1 100 mL 100 mL <br /> 5 mL(MS/MSD) HG-1 <br /> Mercury Standards Preparation <br /> Final Concentration Spiking Standard <br /> Amount Standard Concentration <br /> Calibration Standards: <br /> 0.0002 ppm 0.2 mL HG-2 0.1 ppm <br /> 0.0005 ppm 0.5 mL HG-2 0.1 ppm <br /> 0.001 ppm 1 mL HG-2 0.1 ppm <br /> 0.005 ppm 5 mL HG-2 0.1 ppm <br /> 0.010 ppm 10 mL HG-2 0.1 ppm <br /> ICV Preparation <br /> 0.0025 ppm 2.5 mL HG-1 0.1 ppm <br /> CCV Preparation: <br /> 0.005 ppm 5 mL HG-2 0.1 ppm <br /> Low Level Mercury Standards Preparation <br /> Final Concentration Spiking Standard <br /> Amount Standard Concentration <br /> Calibration Standards: <br /> 0.5 ppt 20 ul HG ICAL 1.0 ppb <br /> 1.0 ppt 40 ul HG ICAL 1.0 ppb <br /> 2 ppt 80 ul HG ICAL 1.0 ppb <br /> 5 ppt 200 ul HG ICAL 1.0 ppb <br /> 10 ppt 400 ul HG ICAL 1.0 ppb <br /> 25 ppt 1000 ul HG ICAL 1.0 ppb <br /> ICV Preparation <br /> 5 ppt 200 ul HG ICV 1.0 ppb <br /> CCV Preparation: <br /> 5 ppt 200 ul HG ICAL 1.0 ppb <br /> Test America North Canton <br /> Revised 1/9/07 <br /> N:\Metals\Preplog.xls <br /> North Canton Page 93 of 137 82 <br />