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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-30534-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-78107 Preparation: 5030B <br /> MS Lab Sample ID: 720-30509-A-2 MS Analysis Batch: 720-78107 Instrument ID: HP12 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 09161024.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 09/16/2010 1849 Final Weight/Volume: 10 mL <br /> Date Prepared: 09/16/2010 1849 <br /> MSD Lab Sample ID: 720-30509-A-2 MSD Analysis Batch: 720-78107 Instrument ID: HP12 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 09161025.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 09/16/2010 1920 Final Weight/Volume: 10 mL <br /> Date Prepared: 09/16/2010 1920 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 93 96 60-140 4 20 <br /> 1,1-Dichloroethane 106 111 60-140 4 20 <br /> Dichlorodifluoromethane 66 64 38-140 3 20 <br /> Vinyl chloride 94 94 58-140 0.3 20 <br /> Chloroethane 101 104 51 -140 3 20 <br /> Trichlorofluoromethane 100 97 60-140 3 20 <br /> Methylene Chloride 103 106 40-140 3 20 <br /> trans-1,2-Dichloroethene 103 107 60-140 4 20 <br /> cis-1,2-Dichloroethene 117 120 60-140 2 20 <br /> Chloroform 116 118 60-140 2 20 <br /> 1,1,1-Trichloroethane 114 118 60-140 3 20 <br /> Carbon tetrachloride 116 118 60-140 2 20 <br /> 1,2-Dichloroethane 125 125 60-140 0.3 20 <br /> Trichloroethene 107 110 60-140 3 20 <br /> 1,2-Dichloropropane 112 113 60-140 0.7 20 <br /> Dichlorobromomethane 135 137 60-140 1 20 <br /> trans-1,3-Dichloropropene 140 138 60-140 1 20 <br /> cis-1,3-Dichloropropene 128 130 60-140 0.8 20 <br /> 1,1,2-Trichloroethane 121 121 60-140 0.1 20 <br /> Tetrachloroethene 107 107 60-140 0.4 20 <br /> Chlorodibromomethane 142 141 60-140 0.6 20 F F <br /> Chlorobenzene 99 99 60-140 0.5 20 <br /> Bromoform 119 117 56-140 1 20 <br /> 1,1,2,2-Tetrachloroethane 101 104 60-140 3 20 <br /> 1,3-Dichlorobenzene 99 101 60-140 2 20 <br /> 1,4-Dichlorobenzene 97 99 60-140 2 20 <br /> 1,2-Dichlorobenzene 100 103 60-140 3 20 <br /> Chloromethane 91 93 52-140 2 20 <br /> Bromomethane 106 105 23-140 0.9 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 90 91 60-140 1 20 <br /> TestAmerica San Francisco Page 18 of 22 <br />