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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-30603-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-78323 Preparation: 5030B <br /> MS Lab Sample ID: 720-30590-A-1 MS Analysis Batch: 720-78323 Instrument ID: HP9 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 09201028.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 09/20/2010 2301 Final Weight/Volume: 10 mL <br /> Date Prepared: 09/20/2010 2301 <br /> MSD Lab Sample ID: 720-30590-A-1 MSD Analysis Batch: 720-78323 Instrument ID: HP9 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 09201029.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 09/20/2010 2334 Final Weight/Volume: 10 mL <br /> Date Prepared: 09/20/2010 2334 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 94 93 60-140 0.6 20 <br /> 1,1-Dichloroethane 100 100 60-140 0.09 20 <br /> Dichlorodifluoromethane 56 55 38-140 3 20 <br /> Vinyl chloride 81 79 58-140 3 20 <br /> Chloroethane 91 89 51 -140 3 20 <br /> Trichlorofluoromethane 95 97 60-140 3 20 <br /> Methylene Chloride 98 100 40-140 2 20 <br /> trans-1,2-Dichloroethene 103 103 60-140 0.5 20 <br /> cis-1,2-Dichloroethene 107 108 60-140 1 20 <br /> Chloroform 101 101 60-140 0.009 20 <br /> 1,1,1-Trichloroethane 107 107 60-140 0.4 20 <br /> Carbon tetrachloride 106 105 60-140 0.8 20 <br /> 1,2-Dichloroethane 95 97 60-140 3 20 <br /> Trichloroethene 98 100 60-140 2 20 <br /> 1,2-Dichloropropane 105 107 60-140 2 20 <br /> Dichlorobromomethane 109 112 60-140 2 20 <br /> trans-1,3-Dichloropropene 106 110 60-140 4 20 <br /> cis-1,3-Dichloropropene 107 110 60-140 2 20 <br /> 1,1,2-Trichloroethane 105 109 60-140 3 20 <br /> Tetrachloroethene 91 92 60-140 0.7 20 <br /> Chlorodibromomethane 108 112 60-140 4 20 <br /> Chlorobenzene 100 101 60-140 0.7 20 <br /> Bromoform 103 108 56-140 5 20 <br /> 1,1,2,2-Tetrachloroethane 103 108 60-140 4 20 <br /> 1,3-Dichlorobenzene 100 101 60-140 1 20 <br /> 1,4-Dichlorobenzene 100 101 60-140 0.7 20 <br /> 1,2-Dichlorobenzene 99 101 60-140 2 20 <br /> Chloromethane 80 79 52-140 0.7 20 <br /> Bromomethane 87 86 23-140 1 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 93 92 60-140 0.9 20 <br /> TestAmerica San Francisco Page 18 of 25 <br />