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Client: Environmental Cost Management, Inc. Quality Control Data TestAmerica Job ID: 720-33784-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 82606/CA LUFTMS - 8260B /CA LUFT MS (Continued) <br /> Lab Sample ID: LCS 720-87521/8 Client Sample ID: LCS 720-87521/8 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 87521 <br /> LCS LCS L <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene 100 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 98 67-130 <br /> Lab Sample ID: LCSD 720-87521/9 Client Sample ID: LCSD 720-87521/9 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 87521 E: <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1-Dichloroethene 25.0 24.4 ug/L 98 64-128 2 20 <br /> 1,1-Dichloroethane 25.0 23.6 ug/L 94 70-130 2 20 <br /> Dichlorodifluoromethane 25.0 19.7 ug/L 79 33-125 1 20 <br /> Vinyl chloride 25.0 24.4 ug/L 98 65-156 1 20 <br /> Chloroethane 25.0 25.4 ug/L 102 62-138 0 20 <br /> Trichlorofluoromethane 25.0 27.3 ug/L 109 74-146 1 20 <br /> Methylene Chloride 25.0 22.5 ug/L 90 73-147 2 20 <br /> trans-1,2-Dichloroethene 25.0 21.4 ug/L 85 75-131 2 20 <br /> cis-1,2-Dichloroethene 25.0 27.8 ug/L 111 70-130 0 20 <br /> Chloroform 25.0 24.7 ug/L 99 70-130 1 20 <br /> 1,1,1-Trichloroethane 25.0 26.5 ug/L 106 70-130 1 20 <br /> Carbon tetrachloride 25.0 26.1 ug/L 104 77-146 1 20 <br /> 1,2-Dichloroethane 25.0 24.0 ug/L 96 70-126 4 20 <br /> Trichloroethene 25.0 24.4 ug/L 98 70-130 1 20 <br /> 1,2-Dichloropropane 25.0 24.0 ug/L 96 70-130 1 20 <br /> Dichlorobromomethane 25.0 27.1 ug/L 109 70-130 2 20 <br /> trans-1,3-Dichloropropene 25.0 27.8 ug/L 111 83-140 3 20 <br /> cis-1,3-Dichloropropene 25.0 26.4 ug/L 106 88-137 4 20 <br /> 1,1,2-Trichloroethane 25.0 25.2 ug/L 101 82-128 6 20 <br /> Tetrachloroethene 25.0 25.3 ug/L 101 70-130 1 20 <br /> Chlorodibromomethane 25.0 28.1 ug/L 112 78-145 5 20 <br /> Chlorobenzene 25.0 25.4 ug/L 102 70-130 0 20 <br /> Bromoform 25.0 27.5 ug/L 110 68-136 6 20 <br /> 1,1,2,2-Tetrachloroethane 25.0 26.4 ug/L 105 70-130 6 20 <br /> 1,3-Dichlorobenzene 25.0 25.7 ug/L 103 70-130 1 20 <br /> 1,4-Dichlorobenzene 25.0 25.4 ug/L 102 87-118 1 20 <br /> 1,2-Dichlorobenzene 25.0 25.5 ug/L 102 70-130 0 20 <br /> Chloromethane 25.0 22.9 ug/L 91 52-175 2 20 <br /> Bromomethane 25.0 25.6 ug/L 103 43-151 0 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 25.1 ug/L 101 42-162 2 20 <br /> ne <br /> EDB 25.0 26.7 ug/L 107 70-130 5 20 <br /> 1,2,4-Trichlorobenzene 25.0 25.7 ug/L 103 70-130 1 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 102 70-130 <br /> 4-Bromofluorobenzene 101 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 100 67-130 <br /> TestAmerica San Francisco <br /> Page 31 of 48 03/23/2011 <br />