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QC Sample Results C <br /> Client: Environmental Cost Management, Inc. TestAmerica Job ID: 720-42018-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 82608 -Volatile Organic Compounds (GUMS) (Continued) <br /> Lab Sample ID: LCSD 720-113241/6 Client Sample ID: Lab Control Sample Dup <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 113241 °/ L <br /> Spike LCSD LCSD Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,2,4-Trichlorobenzene 25.0 23.0 ug/L 92 70-130 2 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 100 70-130 <br /> 4-Bromofluorobenzene 102 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 96 75-138 F <br /> Lab Sample ID: 720-42018-11 MS Client Sample ID: RPS-1 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 113241 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1-Dichloroethene ND 25.0 25.0 ug/L 100 _6_O__140 <br /> 1,1-Dichloroethane ND 25.0 28.3 ug/L 113 60.140 <br /> Dichlorodifluoromethane ND 25.0 20.8 ug/L 83 38.140 <br /> Vinyl chloride ND 25.0 24.3 ug/L 97 58-140 El <br /> Chloroethane ND 25.0 26.9 ug/L 108 51-140 <br /> Trichlorofluoromethane ND 25.0 27.9 ug/L 112 60-140 <br /> Methylene Chloride ND 25.0 27.6 ug/L 110 40-140 <br /> trans-1,2-Dichloroethene ND 25.0 23.6 ug/L 94 60-140 <br /> cis-1,2-Dichloroethene 5.2 25.0 37.8 ug/L 131 60-140 <br /> Chloroform ND 25.0 28.2 ug/L 113 60-140 <br /> 1,1,1-Trichloroethane ND 25.0 28.3 ug/L 113 60-140 <br /> Carbon tetrachloride ND 25.0 28.0 ug/L 112 60-140 <br /> 1,2-Dichloroethane ND 25.0 29.1 ug/L 116 60-140 <br /> Trichloroethene 2.1 25.0 29.5 ug/L 110 60-140 <br /> 1,2-Dichloropropane ND 25.0 28.7 ug/L 115 60-140 <br /> Dichlorobromomethane ND 25.0 30.3 ug/L 121 60-140 <br /> trans-1,3-Dichloropropene ND 25.0 31.0 ug/L 124 60-140 <br /> cis-1,3-Dichloropropene ND 25.0 31.6 ug/L 126 60-140 <br /> 1,1,2-Trichloroethane ND 25.0 30.5 ug/L 122 60-140 <br /> Tetrachloroethene ND 25.0 27.1 ug/L 108 60-140 <br /> Chlorodibromomethane ND 25.0 30.2 ug/L 121 60-140 <br /> Chlorobenzene ND 25.0 27.8 ug/L 111 60-140 <br /> Bromoform ND 25.0 30.0 ug/L 120 56-140 <br /> 1,1,2,2-Tetrachloroethane ND 25.0 30.5 ug/L 122 60-140 <br /> 1,3-Dichlorobenzene ND 25.0 28.0 ug/L 112 60-140 <br /> 1,4-Dichlorobenzene ND 25.0 27.9 ug/L 112 60-140 <br /> 1,2-Dichlorobenzene ND 25.0 27.8 ug/L 111 60-140 <br /> Chloromethane ND 25.0 24.8 ug/L 99 52-140 <br /> Bromomethane ND 25.0 25.7 ug/L 103 23-140 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 25.0 29.8 ug/L 119 60-140 <br /> ne <br /> EDB ND 25.0 29.5 ug/L 118 60-140 <br /> 1,2,4-Trichlorobenzene ND 25.0 23.4 ug/L 94 60-140 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 100 70-130 <br /> 4-Bromofluorobenzene 101 67-130 <br /> TestAmerica Pleasanton <br /> Page 29 of 44 5/15/2012 <br />