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QC Sample Results C <br /> Client: ECM Consultants TestAmerica Job ID: 720-85892-1 <br /> Project/Site: Nestle <br /> Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCSD 440-472969/3 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 472969 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Dibromochloromethane 10.0 11.6 ug/L 116 70-130 2 20 <br /> Methylene Chloride 10.0 9.77 ug/L 98 70-130 6 20 <br /> Tetrachloroethene 10.0 10.6 ug/L 106 70-130 4 20 <br /> trans-1,2-Dichloroethene 10.0 10.1 ug/L 101 70-130 4 20 <br /> trans-1,3-Dichloropropene 10.0 11.6 ug/L 116 70-130 6 20 <br /> Trichloroethene 10.0 10.8 ug/L 108 70-130 5 20 <br /> Trichlorofluoromethane 10.0 10.4 ug/L 104 70-130 2 20 <br /> Vinyl chloride 10.0 10.4 ug/L 104 70-130 6 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichlorobenzene-d4 113 70-130 <br /> 4-Bromofluorobenzene(Surr) 126 70-130 <br /> Lab Sample ID: 720-85892-1 MS Client Sample ID: 110 MANLEY <br /> Matrix: Water Prep Type: Total/NA ❑ <br /> Analysis Batch: 472969 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1,1-Trichloroethane ND H 10.0 10.2 ug/L 102 70-130 <br /> 1,1,2,2-Tetrachloroethane ND H 10.0 9.83 ug/L 98 70-130 <br /> 1,1,2-Trichloroethane ND H 10.0 9.24 ug/L 92 70-130 <br /> 1,1-Dichloroethane ND H 10.0 9.69 ug/L 97 70-130 <br /> 1,1-Dichloroethene ND H 10.0 10.4 ug/L 104 70-130 <br /> 1,2-Dibromoethane(EDB) ND H 10.0 9.30 ug/L 93 70-130 <br /> 1,2-Dichlorobenzene ND H 10.0 10.8 ug/L 108 70-130 <br /> 1,2-Dichloroethane ND H 10.0 9.46 ug/L 95 70-130 <br /> 1,2-Dichloropropane ND H 10.0 10.2 ug/L 102 70-130 <br /> 1,3-Dichlorobenzene ND H 10.0 10.4 ug/L 104 70-130 <br /> Bromodichloromethane ND H 10.0 9.80 ug/L 98 70-130 <br /> Bromoform ND H 10.0 9.63 ug/L 96 70-130 <br /> Bromomethane ND H 10.0 9.20 ug/L 92 70-130 <br /> Carbon tetrachloride ND H 10.0 10.8 ug/L 108 70-130 <br /> Chlorobenzene ND H 10.0 10.1 ug/L 101 70-130 <br /> Chloroethane ND H 10.0 8.52 ug/L 85 70-130 <br /> Chloroform ND H 10.0 9.40 ug/L 94 70-130 <br /> Chloromethane ND H 10.0 8.90 ug/L 89 70-130 <br /> cis-1,2-Dichloroethene ND H 10.0 9.62 ug/L 96 70-130 <br /> cis-1,3-Dichloropropene ND H 10.0 10.4 ug/L 104 70-130 <br /> Dibromochloromethane ND H 10.0 10.8 ug/L 108 70-130 <br /> Methylene Chloride ND H 10.0 8.82 ug/L 88 70-130 <br /> Tetrachloroethene ND H 10.0 10.4 ug/L 104 70-130 <br /> trans-1,2-Dichloroethene ND H 10.0 9.70 ug/L 97 70-130 <br /> trans-1,3-Dichloropropene ND H 10.0 10.6 ug/L 106 70-130 <br /> Trichloroethene ND H 10.0 10.4 ug/L 104 70-130 <br /> Trichlorofluoromethane ND H 10.0 9.67 ug/L 97 70-130 <br /> Vinyl chloride ND H 10.0 8.85 ug/L 89 70-130 <br /> TestAmerica Pleasanton <br /> Page 21 of 35 5/1/2018 <br />