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QC Sample Results C <br /> Client: ECM Consultants TestAmerica Job ID: 720-85956-1 <br /> Project/Site: Nestle <br /> Method: 82608 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCS 720-243063/5 Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 243063 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Trichlorofluoromethane 25.0 25.3 ug/L 101 75-132 <br /> Methylene Chloride 25.0 24.1 ug/L 96 75-128 <br /> trans-1,2-Dichloroethene 25.0 23.4 ug/L 93 79-130 <br /> cis-1,2-Dichloroethene 25.0 21.8 ug/L 87 77-130 <br /> Chloroform 25.0 22.7 ug/L 91 82-130 <br /> 1,1,1-Trichloroethane 25.0 23.6 ug/L 94 81-130 <br /> Carbon tetrachloride 25.0 25.4 ug/L 102 79-133 <br /> 1,2-Dichloroethane 25.0 22.2 ug/L 89 66-132 <br /> Trichloroethene 25.0 25.9 ug/L 104 85-130 <br /> 1,2-Dichloropropane 25.0 22.0 ug/L 88 79-130 <br /> Dichlorobromomethane 25.0 23.8 ug/L 95 81-130 <br /> trans-l,3-Dichloropropene 25.0 23.5 ug/L 94 76-129 <br /> cis-1,3-Dichloropropene 25.0 22.9 ug/L 92 82-130 <br /> 1,1,2-Trichloroethane 25.0 23.1 ug/L 93 80-130 <br /> Tetrachloroethene 25.0 27.5 ug/L 110 81-130 ❑ <br /> Chlorodibromomethane 25.0 25.4 ug/L 101 77-133 <br /> Chlorobenzene 25.0 23.3 ug/L 93 85-130 <br /> Bromoform 25.0 25.4 ug/L 102 79-127 <br /> 1,1,2,2-Tetrachloroethane 25.0 20.6 ug/L 83 70-130 <br /> 1,3-Dichlorobenzene 25.0 23.2 ug/L 93 86-130 <br /> 1,4-Dichlorobenzene 25.0 23.1 ug/L 93 86-130 <br /> 1,2-Dichlorobenzene 25.0 23.4 ug/L 94 85-130 <br /> Chloromethane 25.0 21.2 ug/L 85 46-147 <br /> Bromomethane 25.0 25.7 ug/L 103 65-151 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha 25.0 27.3 ug/L 109 70-145 <br /> ne <br /> EDB 25.0 24.3 ug/L 97 80-130 <br /> 1,2,4-Trichlorobenzene 25.0 25.6 ug/L 102 78-138 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 97 70-130 <br /> 4-Bromofluorobenzene 88 67-130 <br /> 1,2-Dichloroethane-d4(Surr) 90 72-130 <br /> Lab Sample ID: LCSD 720-243063/6 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 243063 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1-Dichloroethene 25.0 23.5 ug/L 94 64-128 1 20 <br /> 1,1-Dichloroethane 25.0 23.1 ug/L 92 77-130 3 20 <br /> Dichlorodifluoromethane 25.0 21.4 ug/L 85 18-173 3 20 <br /> Vinyl chloride 25.0 23.6 ug/L 94 50-156 1 20 <br /> Chloroethane 25.0 24.5 ug/L 98 62-148 1 20 <br /> Trichlorofluoromethane 25.0 24.8 ug/L 99 75-132 2 20 <br /> Methylene Chloride 25.0 24.9 ug/L 99 75-128 3 20 <br /> trans-1,2-Dichloroethene 25.0 23.6 ug/L 95 79-130 1 20 <br /> cis-1,2-Dichloroethene 25.0 22.4 ug/L 90 77-130 3 20 <br /> TestAmerica Pleasanton <br /> Page 9 of 19 4/30/2018 <br />