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QC Sample Results C <br /> Client: ECM Consultants TestAmerica Job ID: 720-86806-1 <br /> Project/Site: Nestle-Ripon <br /> Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCS 440-482428/1002 Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: Total/NA <br /> Analysis Batch: 482428 L <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichlorobenzene-d4 106 70-130 <br /> 4-Bromofluorobenzene(Surr) 102 70-130 <br /> Lab Sample ID: LCSD 440-482428/3 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Water Prep Type: Total/NA • <br /> Analysis Batch: 482428 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1,1-Trichloroethane 5.00 5.16 ug/L 103 70-130 1 20 <br /> 1,1,2,2-Tetrachloroethane 5.00 5.88 ug/L 118 70-130 10 20 <br /> 1,1,2-Trichloroethane 5.00 5.19 ug/L 104 70-130 6 20 <br /> 1,1-Dichloroethane 5.00 5.17 ug/L 103 70-130 0 20 <br /> 1,1-Dichloroethene 5.00 5.12 ug/L 102 70-130 2 20 <br /> 1,2-Dibromoethane(EDB) 5.00 5.37 ug/L 107 70-130 8 20 <br /> 1,2-Dichlorobenzene 5.00 5.35 ug/L 107 70-130 2 20 ❑ <br /> 1,2-Dichloroethane 5.00 5.10 ug/L 102 70-130 4 20 <br /> 1,2-Dichloropropane 5.00 5.04 ug/L 101 70-130 1 20 <br /> 1,3-Dichlorobenzene 5.00 5.32 ug/L 106 70-130 1 20 <br /> Bromodichloromethane 5.00 5.21 ug/L 104 70-130 3 20 <br /> Bromoform 5.00 5.39 ug/L 108 70-130 9 20 <br /> Bromomethane 5.00 5.06 ug/L 101 70-130 2 20 <br /> Carbon tetrachloride 5.00 5.29 ug/L 106 70-130 1 20 <br /> Chlorobenzene 5.00 5.03 ug/L 101 70-130 0 20 <br /> Chloroethane 5.00 4.91 ug/L 98 70-130 4 20 <br /> Chloroform 5.00 5.09 ug/L 102 70-130 2 20 <br /> Chloromethane 5.00 4.91 ug/L 98 70-130 3 20 <br /> cis-1,2-Dichloroethene 5.00 4.86 ug/L 97 70-130 0 20 <br /> cis-1,3-Dichloropropene 5.00 5.36 ug/L 107 70-130 4 20 <br /> Dibromochloromethane 5.00 5.46 ug/L 109 70-130 6 20 <br /> Methylene Chloride 5.00 5.01 ug/L 100 70-130 2 20 <br /> Tetrachloroethene 5.00 5.13 ug/L 103 70-130 1 20 <br /> trans-1,2-Dichloroethene 5.00 4.84 ug/L 97 70-130 0 20 <br /> trans-1,3-Dichloropropene 5.00 5.66 ug/L 113 70-130 7 20 <br /> Trichloroethene 5.00 5.18 ug/L 104 70-130 0 20 <br /> Trichlorofluoromethane 5.00 5.14 ug/L 103 70-130 2 20 <br /> Vinyl chloride 5.00 4.92 ug/L 98 70-130 5 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichlorobenzene-d4 106 70-130 <br /> 4-Bromofluorobenzene(Surr) 103 70-130 <br /> TestAmerica Pleasanton <br /> Page 18 of 28 6/20/2018 <br />