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11 ' 1 10 2nd Aveni ih,YD7,]'achcco,CA 94553-5560 MCCampbell Analytical IDC. Telephone:925-798-1620 Fax:925-798-1622 lilW://www.niccampbell.cem E-mail:main�eomccampbcll coni Ground Zero Analysis,Inc. Client Project ID: #479;Kooyman Date Sampled: 10/01/02 1714 Main Street Date Received: 10/03/02 Client Contact: Greg Stahl Date Extracted: 10/03/02 Esca]on, CA 95320 Client P.O.: Date Analyzed: 10/09/02 Volatiles Organics+Oxygenates by P&T and GC/MS(Basic Target List)* Extraction Method: SW5030B Analytical Method: SW8260B Work Order:0310071 Lab ID i 0210071-001 A Client ID KSD 1-3 - Matrix Soil Compound Concentration * DF °Li-ii Compound Concentration* DF _Acetone ND<250 5.0 50 tert-Amyl methyl ether(TAME) NLK25 5.0 5.0 Benzene ND<25 5.0 5.0 Bromobenzene _ ND<25 5.0 5.0 Bromochloromethane ND<25 5.0 5.0 Bromodichloromethane ND<25 5.0 5._0_ Brvmoform r ND<25 5.0 5.0 Bromomethane ND<25 5.0- 5D 2-Butanone(MEK) ND<50 5.0 10 t-Butyl alcohol(TBA) ND<120 5.025. n-Butyl benzene ND<25 5.0 5.0 sec-Butyl benzene ND<25 5-0 5.0 Cert-Butyl benzene _ ND<25 5A 5.0 Carbon Disulfide ND<25 5.0 5._0 Carbon Tetrachloride ND<25 5.0 5.0 Chlorobenzene ND<25 5.0 5.0 Chloroethane ! ND<25 5.0 5.0 2-Chloroethyl Vinyl Ether ND<50 5.0 10 Chloroform _ I ND<25 5.0 5-0 Chloromethane ND<25 5.0 5.0 2-Chlorotoluene ND<25 5.0 5.0 4-Chlorotoluene ND<25 5.0 -5.0 Dibromochloromethane - ND<25 5.0 5.0 1,2-Dibromo-3-chloropropane ND<50 5.0 10 1,2-1Yibromoetbane-(EDB) ND<25 5-0 5.0 Dibromomethane ND<25 5-0 5.0- 1.2-Dichlorobenzene ND<25 5.0 5.0 1,3-Dichlorobenzene ND<25 5-0 5.0 1,4-Dichlorobenzene ND<25 5.0 5.0 Dichlorodifluoromethane ND<25 5.0 5.0 1,1-Dichloroethane ND<25 5.0 5.0 1,2-Dichloroethane(1,2-DCA) ND<25 5.0 5.0 LI-Dichloroethene ND<25 5.0 5.0 cis-1,2-Dichloroethene - - ND<25 5.0 - 5.0 vans-1,2-Dichloroethene ND<25 5.0 5-0 1,2-Dichloropropane ND<25 5.0 5.0 _ _ - -- _ _ 1,3-Dichloropropane ND<25 5.0 5-0 2,2-Dichloropropane ND<25 5.0 5.0 ]J-Dichloropropene ND<25 1 5.0 i 5.0 cis-1,3-Dichloropropene ND<25 5.0 5.0- trans-1,3-Dichloropropene .0trans-1,3-Dichloropropene ND<25 5.0 j 5.0 Diisopropyl ether(DIPS) ND<25 5.0 5.0 Ethylbenzene ND<25 5.0 5.0 Ethyl tert-butyl ether(ETRE) ND<25 5.0 5.0 Hexachlorobutadiene ND<50 5.0 1 10 2-Hexanone ND<25 5.0 5.0 lodomethane(Methyl iodide) ND<25 5.0 S.0 Isopropylbenzene ND<25 5.0 - 5.0 4-Isopropyl toluene ND<25 5.0 5.0 Methyl-t-butyl ether(MTBE) ND<25 5.0 5.0 Methylene chloride ND<50 5.0 10 4-Methyl-2-pentanone(MIRK) ND<25 5.0 5.0 Naphthalene ! 27 5.0 -1-10 n-Propyl benzene ND<25 5.0 5.0 Styrene ND<25 5.0 5.0 1,1,1,2-Tetrachloroethane ND<25 5.0 5.0 1,1,22-Tetrachloroethane ND<25 5.0 5.0 Tetrachloroethene- ND<25 5.0 5-0 _Toluene 660 1 5.0 5.0 1,2,3-Trichlorobenzene ND<50 5.0 10 1,2,4-Trichlorobenzene ND<50 1 5.0 10 1 1,1,1-Trichloroethane ND<25 5.0 5.0 1,1,2-Trichloroethane ND<25 1 5.0 5.0 . Trichloroethene ND<25 5.0 5.0 Trichlorofluoromethane ND<25 5.0 5.0 1,2,3-Trichl0ropropane ND<25 5.0 5.0 _122,4-Trimethylbenzene 47 5.0 5.0 1,3,5-Trimethylbenzene N1)<25 5.0 5.0 Vinyl Acetate ND<250 5.0 50 Vinyl ChlorideT ND<25 5.0 5.0 -_ --- -- -- - Xvlenes 27 5.0 5.0 Surrogate Recoveries %551: 103 %SS2: --108 -- %SS3: - -- _--- 97.2 Comments: *water and vapor samples and all TCL?&SPLP extracts are reported in uglL,soil/sludge/solid samples in ug/kg, wipe samples in ug/wipe, product/oil/non-aqueous liquid samples in mg/L. ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis. h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than--2 vol.%sediment;j)sample diluted due to high organic content. DHS Certification No. 1644 _� Edward Hamilton,Lab Director