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CURTIS & TOMPKINS SEQUENCE SUMMARY FOR 1014356084 <br /> Instrument : MET26 Begun : 09/04/14 06:44 ' <br /> Method : EPA 6020 SOP Version : icpms rv5 <br /> # File Type Sample ID Matrix Batch Analyzed IDF Stds Uaed ' <br /> 105 14iO4g00105 X XCCB 09/04/14 15:18 1.0 1 <br /> 106 14iO4g00106 CCB 09/04/14 15:23 1.0 1 <br /> 107 14iO4g00107 X RINSE 09/04/14 15:28 1.0 1 ' <br /> 108 14iO4g00108 X RINSE 09/04/14 15:33 1.0 1 <br /> 109 14iO4g00109 X RINSE 09/04/14 15:38 1.0 1 <br /> 110 14iO4g00110 X RINSE 09/04/14 15:43 1.0 1 <br /> 211 14iO4g00111 XBLANK QC755722 Filtrate 214948 09/04/14 16:11 5.0 1 ' <br /> 112 14iO4g00112 CCV 09/04/14 16:16 1.0 13 1 <br /> 113 14iO4g00113 X XCCB 09/04/14 16:21 1.0 1 <br /> 114 14i04900114 CCB B 09/04/14 16:26 1.0 1 ' <br /> 1Filtrate 15 14iO4g00115 LANK QC755722 214948 09/04/14 16:31 5.0 1 <br /> 116 14iO4g00116 -BSQC755723 Filtrate 214948 -6-9/04/14-16.35 5.0 1 <br /> 117 14iO4g00117 BSD QC755724 Filtrate 214948 09/04/14 16:40 5.0 1 <br /> 118 14iO4g00118 MSS 260056-003 Filtrate 214948 09/04/14 16:45 5.0 1 ' <br /> 119 14iO4g00119 MS QC755725 Filtrate i.1-4948 -6-9/04/1416-50 5.0 1 1:CA=21000 <br /> 120 14iO4g00120 MSD QC755726 Filtrate 214948 09/04/14 16:54 5.0 1 1:CA=21000 <br /> 121 14iO4g00121 SAMPLE 260257-001 Filtrate 214948 09/04/14 16:59 5.0 1 2:CA=20000 ' <br /> 122 14i04900122 CCV 09/04/14 17:04 1.0 13 1 <br /> 123 14iO4g00123 X XCCB 09/04/14 17:09 1.0 1 <br /> 124 14iO4g00124 CCB 09/04/14 17:14 1.0 1 <br /> 125 14i04900125 BLANK QC756247 Water 215068 09/04/14 <br /> 126 14iO4g00126 BS QC756248 Water 215068 09/04/14 17:23 5.0 1 <br /> 127 14iO4g00127 BSD QC756249 Water 215068 09/04/14 17:28 5.0 1 <br /> 128 14iO4g00128 MSS 260380-002 Water 215068 09/04/14 17:33 5.0 1 1:NA=67000 ' <br /> 129 14iO4g00129 MS QC756250 Water 215068 09/04/14 17:38 5.0 1 <br /> 130 14iO4g00130 MSD QC756251 Water 215068 09/04/14 17:42 5.0 1 <br /> 131 14iO4g00131 SAMPLE260465-001 Water 215068 09/04/14 17:47 5.0 1 1:NA=22000 <br /> 132 14iO4g00132 SAMPLE 260465-002 Water 215068 09/04/14 17:52 <br /> 133 14iO4g00133 SAMPLE 260465-003 Water 215068 09/04/14 17:57 5.0 1 1:NA=27000 <br /> 134 14iO4g00134 SAMPLE 260465-004 Water 215066 09/04/14 18:01 5.0 1 1:NA=25000 <br /> 135 14i04g00135 CCV 109/04/14 18:06 1.0 13 1 <br /> 136 14104g00136 X XCCB 09/04/14 18:11 1.0 1 ' <br /> 137 14iO4g00137 CCB 09/04/14 18:16 1.0 1 <br /> 138 14iO4g00138 CCV 09/04/14 18:21 1.0 13 1 <br /> 139 14iO4g00139 X XCCB 09/04/14 18:26 1.0 1 ' <br /> 140 14iO4g00140 CCB 09/04/14 18:31 1.6 1 <br /> 141 14iO4g00141 ICSA 09/04/14 18:36 1.0 11 1 8:CA=300000 <br /> 142 14iO4g00142 ICSAB 09/04/14 1840 1.0 12 1 9:CA=300000 <br /> 143 14iO4g00143 X RINSE09/04/14 18:45 1.0 1 ' <br /> 144 14i04900144 X RINSE 09/04/14 18:50 1.0 1 <br /> 145 14iO4g00145 X RINSE 09/04/14 18:55 1.0 1 <br /> 146 14iO4g00146 X RINSE 09/04/14 <br /> 147 14iO4g00147 X RINSE 09/04/14 19:05 1.0 1 <br /> 148 14iO4g00146 X RINSE 09/04/14 19:10 1.0 1 <br /> 149 14iO4g00149 X RINSE 09/04/14 19:15 1.0 1 <br /> 150 14iO4-001 50 X RINSE 09/04/14 19:20 1.0 1 ' <br /> NT 09/05/14 : I verified that the vials loaded on the instrument matched the <br /> sequence data entry, for runs 1 through 150 . ' <br /> Standards used: 1=S24868 2-S25530 3=525103 4=525304 5=S25105 6=S25106 7=525101 66525102 9=825135 10=525529 11=S2S137 <br /> 12=525159 13.525136 14=523905 15=523906 <br /> Page 3 of 3 ' <br /> 101 of 242 ' <br />