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SPLP/TCLP EXTRACTION LOG <br /> ' Curtis & Tompkins,Ltd, <br /> LIMS Batch#: 2)SO S 5 Date/Time ON: q-3-i Z 3 ST Page: 20 <br /> Rotator#'s: 2,jr Tempt(C)ON: 27- Benchbook#: BK3542 <br /> ' Date/Time OFF:°(: --I( 5 Scale Used <br /> Extraction Method: ❑ EPA 1311: TCLP Tempt(C)OFF: 21-Z,( ❑ Leachates <br /> ❑ EPA 1312: SPLP O�Extractions <br /> Sample Free Liq Sieved? Sample pH after Fluid Extract Final <br /> Sam le# SL Mass(g) (yin)+ (yin)* H +1N HC1 # Vol(mL) H *Comments <br /> ' LV---15611 0100 0' I 010000 K.qo <br /> Z'(0vSZI5-00 S P-1 00 ° a P >8.9� l• r1`2000 Ll eS ac,,rcc <br /> 26C 41'1- o er100 0 �S p vr2000 0 <br /> r- a-roo ° 8 P1 113 1 02 °_ <br /> 000 -12 <br /> 5 0 100 0 0 2000❑_ <br /> c 100 ° 0 2000 0 <br /> ' °2000 <br /> ° 100 ° <br /> ciao ° °2000° <br /> ' <br /> 10 0100 ° <br /> °2000° <br /> 0100 0— 0 2000 <br /> ' 0100 0 0 2000 o <br /> 0 _ <br /> 100 0 o 2000 0 <br /> °100 ❑ o 20 Dd` <br /> 5 0100 0 2000❑ <br /> °100 ° I0 2000 0_ <br /> ❑ 100 0 <br /> 112000 0 <br /> 0100 0 n 2000 o <br /> ' 0 100 0 0 2000 0_ <br /> 20 0100 0 0 2000 0 <br /> ° ° 0 2000° <br /> 0 100 0 0 2000 r- <br /> 0100 <br /> _0100 ❑ 0 2000 0 <br /> Temperature Limits: 21 -25 C <br /> 3.5 mL of I N HCl was;added to allsamples bb p ft tp p�3IMS# Date/Initials <br /> ' TCLP Pluid#1 H: 4.88-4.98 su 3 `1 <br /> F Sodium Hydroxide(NaOH) 'Stoijl'� N�Z2r} DD <br /> TCLP Fluid#2 pH: 2.83-3.03 su Acetic acid(HOAc) 11 E 1'g <br /> SPLP Fluid#I pH: 4.15-425 su Fluid#1 pH,Prep Date y-15 Ab F-U-11 ct-3-11 <br /> SPLP Fluid#2 pH: 4.95-5.05 su Fluid#2 pH,Prep Date r— <br /> Hot Plate Thermometer(Temperature,Serial#) IZ�o °C 11 <br /> Extract filtered throngh 0.?um x 142mm TCLP filter pap J e�00 3 o 25 <br /> Metals extracts acidified to pH Q with I mL HNO3 5 <br /> Extra 'on Chemist Date Reviewed Online/See LIMS <br /> ' 132 of 242 <br />