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Kennedy/Jenks Consultants <br /> Appendix B: Groundwater Sampling and Analysis Plan <br /> This Groundwater Sampling and Analysis Plan (SAP) will be used as a guidance document for <br /> individuals responsible for conducting groundwater monitoring and sampling activities in conjunction <br /> with the Hydrogeologic Investigation Work Plan for the Sutter Home Lodi Winery. <br /> BA Analytical Methods, Sample Containers and Preservatives <br /> For the first several months of 2010, depth to groundwater will be measured monthly in monitoring <br /> wells GW-1 through GW-14, to obtain data on groundwater gradient and velocity. In accordance <br /> with the MRP, samples from groundwater monitoring wells GW-1 through GW-14 will be analyzed <br /> quarterly for ammonia, boron, bromoform, bromodichloromethane, chloride, chloroform, <br /> dibromochloromethane, electrical conductivity, fixed dissolved solids, iron, manganese, nitrate, <br /> sodium, total dissolved solids, total Kjeldahl nitrogen, and total nitrogen. For the first two quarters of <br /> 2010, the monitoring well samples will also be analyzed for alkalinity, bicarbonate, calcium, <br /> carbonate, hardness, hydroxide, magnesium and sulfate. Samples from wells DWS-1 through <br /> DWS-3 will be analyzed for nitrate and total dissolved solids for two quarters. Table 6.1 outlines the <br /> analytical methods, associated reporting limits, sample containers and preservatives for these <br /> analyses. <br /> TABLE B.1 — ANALYTICAL PROTOCOLS <br /> Reporting Con- Sample Holding <br /> Constituent Test Method Limit (mg/1) tainer Volume Preservative(') Time <br /> Total Alkalinity as EPA 310.1 1.0 P 250 ml None 14 days <br /> Calcium Carbonate <br /> (CaCO3) <br /> Ammonia(as NH4) <br /> Bicarbonate(HCO3) EPA 310.1 1.0 P 250 ml None 14 days <br /> Boron(B) <br /> Bromoform <br /> Bromodichloromethane <br /> Calcium (Ca) EPA 6010 0.5 P _ 250 ml _ HNO3 pH<2 6 months <br /> Carbonate (CO3) EPA 310.1 1.0 P 250 ml None 14 days <br /> Chloride(Cl) EPA 300.0 0.2 P 250 ml None 28 days <br /> Chloroform <br /> Di bromochloromethan e <br /> Electrical Conductivity EPA 120.1 1 (umhos/cm P 250 ml None 28 days <br /> (EC) (M 25°C) <br /> Fixed Dissolved Solids <br /> (FDS) <br /> Hardness EPA 130.2 3.3 P 250 ml HNO3 6 months <br /> Hydroxide(OH) EPA 310.1 1.0 P 250 ml None 14 days <br /> Iron (Fe) <br /> Magnesium (Mg) EPA 6010 0.5 P 250 ml HNO3 pH<2 6 months <br /> Manganese(Mn) <br /> Nitrate-Nitrogen EPA 300.0 0.1 P 250 ml None 48 hours <br /> (NO3 as N) <br /> pH EPA 0.1 unit P 250 ml None 24 hours <br /> 9040B/9045C <br /> Sodium (Na) EPA 6010 0.5 P 250 ml HNO3 pH<2 6 months <br /> Hydrogeologic Investigation and Groundwater Sampling and Analysis Work Plan B-1 <br /> Sutter Home Lodi Winery, Lodi, California <br /> gtifyrwpletlmN4ablg6�g6660g5.06_rvlhrhana109+epart51w9 WkSAWyh x P1W4ppentlics ppb .0.pp,&-b .p,tl <br />