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1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> McCampbell Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax;(925)252-9269 <br /> "When Quality Counts" I hnp://www..e.pbsllxom/E-mad:mam@f =pbelloom <br /> Quality Control Report <br /> Client: Neil O.Anderson&Associates WorkOrder: 1404047 <br /> Date Prepared: 4/1/14 BatchlD: 88846 <br /> Date Analyzed: 4/2/14 Extraction Method: SW5030B <br /> Instrument: GC10 Analytical Method: SW8260B <br /> Matrix: Soil Unit: mg/Kg <br /> Project: 4LZ140001;NOA Drywell,Lodi,CA Sample ID: MB/LCS-88846 <br /> 1403591-018AMS/MSD <br /> QC Summary Report for SW8260B <br /> Analyte MS MSD SPK SPKRef MS MSD MSIMSD RPD RPD <br /> Result Result Val Val %REC %REG Limits Limit <br /> tert-Amyl methyl ether(TAME) 0.04337 0.04598 0.050 ND 86.7 92 70-130 5.82 30 <br /> Benzene 0.04766 0.04989 0.050 ND 95.3 99.8 70-130 4.57 30 <br /> t-Butyl alcohol(TBA) 0.1986 0.2126 0.20 ND 99.3 106 70-130 6.80 30 <br /> Chlorobenzene 0.04911 0.05135 0.050 ND 98.2 103 70-130 4.46 30 <br /> 1,2-Dibromoethane(EDB) 0.05068 0.05156 0.050 ND 101 103 70-130 1.72 30 <br /> 1,2-Dichloroethane(1,2-DCA) 0.04387 0.04556 0.050 ND 87.7 91.1 70-130 3.78 30 <br /> 1,1-Dichloroethene 0.03681 0.0407 0.050 ND 73.6 81.4 70-130 10.1 30 <br /> Diisopropyl ether(DIPE) 0.04399 0.04559 0.050 ND 88 91.2 70-130 3.58 30 <br /> Ethyl lert-butyl ether(ETRE) 0.04347 0.0459 0.050 ND 86.9 91.8 70-130 5.45 30 <br /> Methyl-t-butyl ether(MTBE) 0.04517 0.04775 0.050 ND 90.3 95.5 70-130 5.56 30 <br /> Toluene 0.05187 0.0535 0.050 ND 104 107 70-130 3.08 30 <br /> Trichloroethene 0.04728 0.04957 0.050 ND 94.6 99.1 70-130 4.73 30 <br /> Surrogate Recovery <br /> Dibromofluoromethane 0.1704 0.1719 0.18 97 98 70-130 0.913 30 <br /> Toluene-0 0.1629 0.1621 0.18 93 93 70-130 0 30 <br /> 4-BFB 0.01717 0.01764 0.018 98 101 70-130 2.72 30 <br /> CDPH ELAP 1644♦NELAP 4033ORELAP " QA/QC Officer <br /> Page 46 of 78 <br />