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01 <br /> McCampbell Analytical, Inc. "'^W�°wFeee877)252-926 /F.:(9565-17-9 <br /> Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> °When Quality Counts" http://wo,, m.c.pbdl o./E-mail:mein@mccwpbell.com <br /> Quality Control Report <br /> Client: Neil O.Anderson&Associates WorkOrder: 1404047 <br /> Date Prepared: 4/3/14 BatchlD: 88945 <br /> Date Analyzed: 4/3/14 Extraction Method: SW5030B <br /> Instrument: GC3 Analytical Method: SW802113/8015Bm <br /> Matrix: Water Unit: n/L <br /> Project: #LZ140001;NOA Drywell,Lodi,CA Sample ID: MB/LCS-88945 <br /> 1404047-008AMS/MSD <br /> QC Summary Report for SW8021B/8015Bm <br /> Analyte MB LCS RL SPK MB LCS LCS <br /> Result Result Val SS%REC %REC Limits <br /> TPH(btex) ND 58.91 40 60 - 98.2 70-130 <br /> MTBE ND 9.735 5.0 10 - 97.3 70-130 <br /> Benzene ND 9.777 0.50 10 - 97.8 70-130 <br /> Toluene ND 9.862 0.50 10 - 98.6 70-130 <br /> Ethylbenzene ND 9.763 0.50 10 - 97.6 70-130 <br /> Xylenes ND 29.41 0.50 30 - 98 70-130 <br /> Surrogate Recovery <br /> aaa-TFT 9.577 9.432 10 96 94 70-130 <br /> Analyte MS MSD SPK SPKRef MS MSD MS/MSD RPD RPD <br /> Result Result Val Val %REC %REC Limits Limit <br /> TPH(btex) 59.61 60.42 60 ND 99.3 101 70-130 1.35 20 <br /> MTBE 10.4 10.68 10 ND 104 107 70-130 2.66 20 <br /> Benzene 10.5 10.58 10 ND 105 106 70-130 0.736 20 <br /> Toluene 10.63 10.65 10 ND 106 107 70-130 0.228 20 <br /> Ethylbenzene 10.63 10.64 10 ND 106 106 70-130 0 20 <br /> Xylenes 31.99 31.9 30 ND 107 106 70-130 0.288 20 <br /> Surrogate Recovery <br /> aaa-TFT 9.777 9.91 10 98 99 70-130 1.35 20 <br /> CDPH ELAP 1644♦NELAP 4033ORELAP " QA/QC Officer <br /> Page 58 of 78 <br />