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NOA Drywell Closure and Investigation Page 9 of 26 <br /> ' May 30, 2014 <br /> sample was collected from drywell 1 at sixty (60) feet bgs and split between two (2) identical <br /> sampling containers for Replicate Samples Quality Assurance/Quality Control purposes. For <br /> drywell 2, groundwater was first encountered at 58.5 feet bgs. Soil samples were collected at <br /> fifty-five (55) and sixty (60) feet bgs. The total number of soil samples collected from the <br /> drywells is thirteen (13). The drywell and sampling locations are shown on Plate 6 and Plate <br /> 7, Appendix A. <br /> 4.3 Sampling Equipment and Collection Methods <br /> Field exploration was performed under the supervision of a California Professional Geologist <br /> and/or Engineer. A geologist experienced with investigation and remediation of chemical <br /> releases at commercial properties was present during sampling and drilling to perform sample <br /> collection, maintain logs of the boring, and make observations of site conditions. Groundwater <br /> and soil samples were collected by NOA under the supervision and oversight of EHD. <br /> 4.3.1 Groundwater <br /> A 36-inch long disposable bailer was used to sample groundwater from the drywells. No <br /> separate floating phase was observed while sampling. A clean disposable bailer was lowered <br /> into the wells to collect groundwater and then emptied into the appropriate sampling bottles as <br /> detailed below. The groundwater sampling equipment and collection methods described below <br /> for each drywell are listed in sequential sampling order. <br /> Two (2) pre-chilled, pre-labeled 40-ml VOA vials with a Teflon septum lid were filled for volatile <br /> organics testing. Two (2) vials are required for one VOA sample. The samples were preserved <br /> with hydrochloric acid. The VOA vials were filled completely at a rate of less than 100 milliliters <br /> per minute to prevent the presence of headspace. The lid with the Teflon septum was tightened <br /> j onto the vial. The vial was turned upside down and tapped to check for the presence of air <br /> bubbles. The sample was recorded, labeled and stored at a temperature of approximately 4°C <br /> in an ice chest for transportation to the analytical laboratory. <br /> One (1) pre-labeled, one-liter amber glass bottle with a Teflon septum was filled for semi- <br /> volatile organics testing. Collection methods specified for volatile organics were followed. The <br /> sample was recorded, labeled and stored at a temperature of approximately 4°C in an ice chest <br /> for transportation to the analytical laboratory. <br /> One (1) pre-labeled, polyethylene, certified metal-free bottles were filled for metals testing for <br /> each well. In addition, two (2) pre-labeled, polyethylene, certified metal-free bottles were filled <br /> from groundwater from DW-2 for Replicate Samples Quality Assurance/Quality Control purposes <br /> ' (See Section 4.5). No preservatives were added since the samples will be analyzed for Mercury. <br /> Samples were analyzed within the holding time. The samples were recorded, labeled and stored <br /> at a temperature of approximately 4°C in an ice chest for transportation to the analytical <br /> laboratory. <br /> Two (2) pre-chilled, pre-labeled 40-ml VOA vials with Teflon septa were filled for Total <br /> Petroleum Hydrocarbons (TPH) as Gasoline testing. The sample was preserved with <br /> hydrochloric acid. Collection methods specified for volatile organics were followed. The sample <br /> 902 Industrial Way• Lodi, CA 95240• 209.367.3701 • Fax 209.333.8303 02014 Neil 0. Anderson&Associates, Inc. <br />