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laboratories <br /> ATC Associates, Inc <br /> 1117 Lone Palm Ave, Suite B Blank!QC Data <br /> Modesto, CA 95351 Method 8015M/8021B/8260B <br /> Prot 10 54 62596 0001 Matrix Water <br /> Site Farmer Property <br /> _ Method Rep Lim <br /> Sample ID Blank Water Soil <br /> Units uglL uglL mg/Kg <br /> Method 8015M 180218 Date Analyzed 03/11/05 <br /> Total Petroleum Hydrocarbons <br /> @ Gasoline <50 50 10 <br /> Benzene <0 5 0 5 0 005 <br /> Toluene <0 5 0 5 0 005 <br /> Xylenes <1 0 1 0 0 010 <br /> Ethyl Benzene <0 5 0 5 0 005 <br /> Surrogate Spike Recovery 90% <br /> Method 82608 Date Analyzed 03/08/05 <br /> t-Butanol(TBA) <5 0 5 0 0 050 <br /> Methyl-t-Butyl Ether(MTBE) <0 5 0 5 0 005 <br /> . Di-Isopropyl Ether(DIPE) <0 5 0 5 0 005 <br /> Ethyl-t-Butyl Ether(ETBE) <0 5 0 5 0 005 <br /> t-Amy!Methyl Ether(TAME) <0 5 0 5 0 005 <br /> 1,2-Dichloroethane(1,2-DCA) <0 5 0 5 0 005 <br /> 1,2-Dibromoethane(EDB) <0 5 0 5 0 005 <br /> Surrogate Spike Recovery 92% <br /> Matrix Spike Recovery Summary <br /> Method Lab ID Client ID Analyte %Recovery RPD <br /> MS 1 MSD <br /> 8015M F03135 MW5 Gas 88180 10 <br /> 8260E F03140 MW10 ETBE 1121102 9 <br /> Laboratory Control Spike Recovery Summary <br /> Method LCSID ID Analyte Percent <br /> Recovery <br /> 8021 B LCS0311 F Ethyl Benzene 85 <br /> 82608 LCS0308F DIPE 99 <br /> Note(s) <br /> . Water samples are reported in uglL soillsludge samples in mg/Kg,productlodlnon-aqueous liquid samples in mg/L <br /> NO means not detected at or above the stated reporting limit,NIA means analyte not applicable to this analysis <br /> 2905 Roilrood Avenue Cores CA 95307 v Prone (209) 581 -9280 e Fox (209) 581 -9282 <br /> emoll info@orgonlobs corn <br />