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y <br />inorganic Section <br />I -IML NUIT-finer: AN075 <br />Quality Assurance <br />Summary <br />for 1CP <br />to ANO 1575 <br />(di <br />i <br />N <br />M <br />� <br />HML Soil QC Sample <br />Method <br />Calibration Verification <br />O <br />M <br />Element <br />Blank <br />Standard <br />Dupfrcafe Spiked <br />Sarn k <br />P <br />HML No-: AN0141a <br />Matrix; <br />41 <br />o <br />mg/kg <br />SOfL <br />mglL <br />Spike <br />Results <br />m Ik <br />3 9 <br />Unspiked Spike <br />O <br />found <br />known <br />% <br />found <br />known <br />;{, <br />Aesuft <br />Added <br />%Recovery <br />m <br />As -Arsenic. <br />57.9 <br />mg/kq <br />A: <br />8: <br />Ri'Q <br />(mglkgl <br />(mg/kg] <br />A: <br />B' <br />o <br />Ba-r3arium <br />4-4.4 <br />68.2 <br />50.6 <br />84.9 <br /><0.10 <br />9. 88 <br />10.0 <br />98.6 <br />195 <br />193 <br />4.35 <br />u <br />z <br />Be Elaryliium <br />3,75 <br />4.1 i <br />87.7 <br /><0.010 <br />9.6 i <br />10-0 <br />96.3 <br />192 <br />191 <br />148 <br />50.0 <br />94.0 <br />90.0 <br />Cd -Cadmium <br />17.0 <br />19.3 <br />91.2 <br /><0.005 <br />10.1 <br />10.0 <br />101 <br />5.50 <br />5-5 <br />744 <br />50.0 <br />94.0 <br />Cc Cohaft <br />19.5 <br />21.9 <br />88.1 <br /><0.OTO <br />10.2 <br />10.0 <br />i 02 <br />207 <br />206 <br />206 <br />2.15 <br />68.2 <br />10.0 <br />7066.0 <br />106 <br />112 <br />112 <br />Cr Chromium <br />7.2.9 <br />25.7 <br />89.0 <br /><0.05 <br />10-1 <br />70.0 <br />101 <br />123 <br />723 <br />1 23 <br />0.00 <br />7 60 <br />50.0 <br />54.0 <br />92.0 <br />d <br />-a <br />Cu -Copper <br />171 <br />89.7 <br /><0.08 <br />10.2 <br />10.0 <br />i02 <br />i63 <br />16i <br />75.7 <br />50.0 <br />94.6 <br />94.6 <br />� <br />Mo -Molybdenum <br />15.6 <br />124 <br />80.5 <br /><0.10 <br />9.74 <br />10.0 <br />658 <br />658 <br />4.17 <br />714 <br />50.0 <br />98.0 <br />94.0 <br />Ni -Nickel <br />21.2 <br />18.0 <br />86.7 <br /><0.10 <br />10.1 <br />10.0 <br />101 <br />101 <br />125 <br />123 <br />0.00 <br />156 <br />500 <br />100 <br />i00 <br />"-' <br />- <br />Pb-Lcad <br />24.0 <br />88.3 <br /><0.05 <br />]0.2 <br />10.0 <br />102 <br />217 <br />217 <br />4.04 <br />74.5 <br />50.0 <br />101 <br />97.0 <br />3 <br />Se-Se(eniurn - <br />22.6 <br />56.6 <br />27.7 <br />82=4 <br /><0-10 <br />10.2 - <br />T 0.6 <br />102 <br />148 <br />147 <br />a.o0 <br />i 70 <br />TI -Thallium <br />78.9 <br />67.0 <br />84.5 <br /><0.15 <br />9.89 <br />10.0 <br />98.9 <br />177 <br />177 <br />2.15 <br />101 <br />50.0 <br />94.0 <br />92.0 <br />_ <br />V -Vanadium <br />88.4 <br />69.3 <br /><0A5 <br />10-0 <br />10.0 <br />100 <br />155 <br />0.00 <br />127 <br />50'0 <br />100 <br />100 <br />Zn -Zinc. <br />34.3 <br />38.6 <br />88.9 <br /><0.06 <br />9.94 <br />10.0 <br />954 <br />168 <br />157 <br />4.17 <br />T08 <br />50.0 <br />94.0 <br />98.0 <br />123 <br />141 <br />87.2 <br />0.1Q <br />10,2 <br />TO.O <br />102 <br />400 <br />7 65 <br />Ci -45 <br />120 <br />50.0 <br />98.0 <br />90.0 <br />HML Liquid QC Sample <br />Rl <br />Reagent <br />Environmental Express <br />410 <br />185 <br />351 <br />50.0 <br />98.0 <br />118 <br />Element <br />Blank <br />QC7 & <br />DC 19 <br />Duplicate <br />A Spiked <br />Sample <br />HML NO.: <br />AN0157s <br />Matrix: <br />= <br />mg/kg <br />Reference Standards <br />LIQUID <br />found <br />m IL <br />Spike Results <br />mg/kg <br />9 g <br />Unspiked <br />Spice <br />% Recovery <br />known <br />% <br />mglL <br />found <br />known <br />g6 <br />A; <br />Aesuft <br />Added <br />Cr) <br />�- <br />As -Arsenic <br />2.49 <br />2.63 <br />94.7 <br /><0.10 <br />B: <br />RPD <br />imglkg] <br />fmg/kg} <br />A: <br />B. <br />C) <br />Ba -Barium <br />9.55 <br />9.92 <br />96.3 <br /><0.010 <br />1.00 <br />0.98 <br />1.00 <br />? 00 <br />48.4 <br />48.2 <br />0.41 <br /><T.00 <br />50.0 <br />96.8 <br />Q <br />� <br />Be-Serylfium <br />2.9fi <br />2.97 <br />99.7 <br /><0.005 <br />1 AO <br />98.0 <br />49.3 <br />�0 <br />O.42 <br />O.33 <br />50.0 <br />96.4 <br />Cd -Cadmium <br />3.02 <br />3.10 <br />97.4 <br /><0.010 <br />1.01 <br />T.00 <br />101 <br />10.3 <br />3 <br />0.00 <br /><0.05 <br />10.0 <br />97.9 <br />47.5 <br />J <br />Q <br />;o CobaFt <br />2.64 <br />2.66 <br />99.2 <br /><0.05 <br />i .04 <br />1.00 <br />7 04 <br />50.9 <br />50.5 <br />0.99 <br /><0.10 <br />50.0 <br />103 <br />103 <br />ul <br />n <br />v <br />Cr -Chromium <br />5,1 <br />15.0 <br />101 <br />1 •p3 <br />1-� <br />103 <br />51.2 <br />50.9 <br />0.00 <br /><0-50 <br />i 02 <br />1 O1 <br />CU -Co per <br />69.5 <br />fi6.1 <br />105 <br /><0.08 <br />1,03 <br />9.00 <br />703 <br />50.5 <br />50.1 <br />T_00 <br /><0.80 <br />50.0 <br />102 <br />102 <br />0 <br />0 <br />E <br />MO -Molybdenum <br />6.26 <br />6.36 <br /><0.10 <br />7.02 <br />1 AO <br />102 <br />59.1 <br />55.7 <br />8.50 <br />50.0 <br />101 <br />] 00 <br />W <br />CE <br />Ni Nickel <br />11.5 <br />98.4 <br /><0.10 <br />1.03 <br />1.00 <br />103 <br />51-6 <br />51-2 <br />17.6 <br />50.0 <br />83.0 <br />76.2 <br />07 <br />Pb -Lead <br />6.38 <br />11.7 <br />98.3 <br /><0.05 <br />9.03 <br />1.00 <br />103 <br />50.3 <br />50.5 <br />0.98 <br /><1_00 <br />50.0 <br />103 <br />102 <br />Cn <br />Se -Selenium <br />14.3 <br />6.18 <br />103 <br />< 0.10 <br />1.05 <br />i .00 <br />105 <br />50-0 <br />49.5 <br />0.99 <br /><0.50 <br />50.0 <br />102 <br />101 <br />TI -Thallium <br />31}.7 <br />14.1 <br />101 <br /><0.15 <br />i .00 <br />1.00 <br />100 <br />48.9 <br />¢8,g <br />1.0 9 <br />< 1.00 <br />50.0 <br />100 <br />99.0 <br />C <br />V -Vanadium <br />34.5 <br />101 <br /><0.15 <br />0.98 <br />7.00 <br />98.0 <br />54.5 <br />54.6 <br />0 20 <br />< 1-50 <br />50.0 <br />97,8 <br />97.6 <br />cv <br />Zn -Zinc <br />2.35 <br />2.33 <br />701 <br /><0.06 <br />1.00 <br />1.00 <br />100 <br />48.7 <br />0.00 <br /><1.50 <br />50.0 <br />F09 <br />709 <br />N <br />24.7 <br />24,4 <br />lOT <br /><0.10 <br />1.03 <br />T_00 <br />103 <br />48.4 <br />0.62 <br /><0.60 <br />50.0 <br />97.4 <br />96.8 <br />}:P <br />Analyst's Signature; <br />52.7 <br />51.6 <br />i .80 <br />2.52 <br />50 0 <br />i� <br />98.2 <br />Q hemist: Fatima <br />- <br />Flussain <br />Chemist's Si <br />Jamail <br />Garcha, Speciafist�_ <br />7 <br />nate <br />Analyzed:-- 05/20144 <br />- <br />-grtature: <br />Date: <br />N <br />