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September 23, 2008 Lab ID : STKO838541 Luhdorff& Sealmanini Consulting Customer : 3-12023 Quality Control - Inorganic Constituent Method Date/ID T.Npe Units Conc. QC Data DQO Note Wet Chem Fluoride 300.0 08/27/2008:208662 MSRPD mg/L 100.0 105% :578-137 LCS mg/L 2.500 108% 90-110 MS mg/L 50.00 112% 81-126 (CH 0877644-001) MSD mg/L 50.00 114% 81-126 MSRPD mg/L 100.0 1.3% :512.1 300.0 08/27/2008:210326 CCB ppm 0.000 0.1 CCV ppm 2.500 108% 90-110 CCB ppm 0.000 0.1 CCV ppm 2.500 110% 90-110 CCB ppm 0.000 0.1 CCV ppm 2.500 109% 90410 CCB ppm 0.000 0.1 CCV ppm 2.500 108% 90-110 CCB ppm 0.000 0.1 CCV PPM 2.500 110% 90-110 Hydroxide 2320B 08/29/2008:208758 Dup mg/L 0.0 10 2320B 09/02/2008:208824 Dup mg/L 0.0 l0 2320B 09/03/2008:208866 Dup m 0.0 10 MBAS 5540C 08/27/2008:208654 MS mg/L 1.000 100% 90-110 (SP 0809339-001) MSD mg/L 1.000 100% 90-110 MSRPD m 1.000 1 0.0 :_0.1 5540C 08/27/2008:210230 CCB mg/L 0.000 0.1 CCV mg/L 1.000 100% 99-101 Nitrate 300.0 08/27/2008:208662 LCS mg/L 20.00 95.9% 90-110 (STK0838664-001) MSD mg/L 400.0 99.9% 88-124 MSRPD mg/1. 100.0 105% :_78-137 LCS mg/L 20.00 102% 90-110 MS mg/L 400.0 103% 88-124 (CH 0877644-001) MSD mg/L 400.0 104% 88-124 MSRPD m 100.0 1 1.2% :_29.1 300.0 08/27/2008:210326 CCB ppm 0.000 0.4 CCV ppm 20.00 97.0% 90-110 CCB ppm 0.000 0.4 CCV ppm 20.00 100% 90-110 CCB ppm 0.000 0.4 CCV ppm 20.00 101% 90-110 CCB ppm 0.000 0.4 CCV ppm 20.00 96.5% 90-110 CCB ppm 0.000 0.4 CCV PPM 20.00 99.3% 90-110 Nitrite 300.0 08/27/2008:208662 LCS mg/L 15.00 105% 90-110 (STK0838664-001) MSD mg/L 300.0 103% 91-121 MSRPD mg/L 100.0 105% 578-137 LCS mg/L 15.00 110% 90-110 MS mg/L 300.0 104% 91-121 (CH 0877644-001) MSD mg/L 300.0 106% 91-121 MSRPD mg/L 100.0 1.6% :523.8 000) 08/27/2008:210326 CCB ppm 0.000 0.3 CCV ppm 15.00 108% 90-110 CCB ppm 0.000 0.3 CCV ppm 15.00 109% 90-110 CCB ppm 0.000 0.3 CCV ppm 15.00 110% 90-110 CCB PPM 1 0.000 0.3