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1 <br /> 1 <br /> AL�'ORNIA € :AGORA RYSERVICESEnvironmental,, Chemic <br /> Analysis Report: Volatile Organic Compounds by GC/MS,l EPA;:Method 8260B <br /> Client: CRWQCB - Sacramentoj <br /> Pro j ec t No.!!: <br /> 3443 Routier Road Contacd: Jim Barton <br /> Sacramento, CA 95827 :1Phone: (916)255-3115 <br /> Project: 420 W. Kettleman Rd Lodi <br /> Lab Contact: Ray Oslowski <br /> ! Lab ID No:': U4094-2A <br /> Date Sampled: 12/19/2002 Job No:: 854094 <br /> Date Received: 12/19/2002 COC Log No! : 28467 <br /> Date Extracted: N/A Batch No!!: 34109 <br /> Date Analyzed: 12/26/2002 Instrument TD: M502 <br /> Daae Reported: 12/31/2002 Analyst ID: ROGERY <br /> Client ID No. : TB-1 Matrix: WATER f <br /> `• SURROGATE <br /> F <br /> Surrogate <br /> Analyte Results Surr Cone. Recovery'; Lower Spec Upper Spec <br /> CAS No. (ug/L) (ug/L) (percent') (Limit) (Limit) <br /> 1,2-Dichloroethane-d4 <br /> N/A 48 .7 50. 0 97 1 66 135 <br /> j Toluene-d8 <br /> N/A 57.2 50.0 114 72 125 <br /> p-Bromofluorobenzene <br /> 460004 56 .2 50.0 112 I 73 125 <br /> TB-1 i <br /> Results Rep. Limit Dilution <br /> Analyte CAS No. (ug/L) (ug/L) (factor) <br /> I '1 <br /> Acetone 67641 ND 100 1.0 <br /> Benzene 71432 ND 5 . 0 1. 0 } <br /> Bromobenzene 108861 ND ' 5. 0 1. 0 <br /> Bromochloromethane 74975 ND 5 . 0 1. 0 <br /> Bromodichloromethane 75274 ND I 5.0 1. 0 <br /> Bromoform 75252 ND 5.0 1.0 <br /> Bromomethane 74839 ND ; 10 1.0 I <br /> 2-Butanone 78933 ND 100 1.0 <br /> n-Butylbenzene 104518 ND 5.0 1.0 <br /> sec-Butylbenzene 135988 ND 5. 0 1. 0 <br /> tert-Butylbenzene 98066 ND ; 5 . 0 1. 0 <br /> Carbon tetrachloride 56235 ND 5 .0 1. 0 i <br /> Chlorobenzene 108907 ND 5.0 1. 0 <br /> Chloroethane 75003 ND I 10 1. 0 <br /> Chloroform 67663 ND 5 .0 1. 0 <br /> Chloromethane 74873 ND 10 1. 0 <br /> o-Chlorotoluene 95498 ND ; 5.0 1. 0 <br /> p-Chlorotoluene 106434 ND 5.0 1. 0 <br /> Dibromochloromethane 124481 ND 5. 0 1. 0 <br /> Dibromomethane 74953 ND 5.0 1.0 <br /> 1,2-Dibromo-3-chloropropane 96128 ND 10 1. 0 <br /> 1,2-Dichlorobenzene 95501 ND 5 .0 1. 0 <br /> 1, 3-Dichlorobenzene 541731 ND " 5 .0 1. 0 <br /> 1,4-Dichlorobenzene 106467 ND 5.0 1. 0 <br /> Dichlorodifluoromethane 75718 ND 10 1.0 <br /> 1,1-Dichloroethane 75343 ND 5 .0 1. 0 I <br /> 1,2-Dichloroethane 107062 ND .5 .0 1. 0 <br /> 1, 1-Dichloroethene 75354 ND 5.0 1. 0 <br /> cis-1,2-Dichloroethene 156592 ND 5.0 1. 0 <br /> trans-1,2-Dichloroethene 156605 ND. 5.0 1. 0 <br /> ND = Not detected at or above indicated Reporting Limit 1 <br /> ;3 1 <br /> CA DONS E1:A2 Accreditation/Registration Humber 1233 f <br /> 11 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 .800-638-7301 916-638-7301 Fax: 916-638-4510 <br />