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t <br /> Petroleum Hydrocarbons (TPH, modified EPA 8015) , benzene, <br /> ethylbenzene, toluene and xylenes (BTEX, FPA method 8020) . Selected <br /> soil samples were analyzed for total lead using EPA Method 7421. <br /> 3.0 QUALITY ASSURANCE PLAN <br /> 3.1 General Sample COUGction and .Randling Procedures <br /> Proper collection and handling are essential to ensure the quality of <br /> a sample. Each sample was collected in a suitable container, preserved <br /> correctly for the intended analyses, and stored prior to analysis for <br /> no longer than the maximum allowable holding time. Details on the <br /> -- procedure for collection and handling of soil samples to be used on <br /> this project can be found in section 1.0 (Methods) . <br /> 3.2 Sample Identification and chain-of-Custody Procedures. <br /> Sample identification and chain-of-custody procedures ensure sample <br /> integrity and document sample possession from the time of collection <br /> to its ultimate disposal. Each sample container submitted analysis was <br /> affixed with a label to identify the job number, date, and time of <br /> _ sample collection, and a sample number unique to that sample. This <br /> information, in addition to a description of the sample, field mea- <br /> surements made, sampling methodology, names of on-site personnel, .and <br /> any other pertinent field observations were recorded on the borehole <br /> �., log in the field records. All samples were analyzed by a State- <br /> certified laboratory. <br /> -, A chain-of-custody form was ed to record possession of the sample <br /> i from time of collection to `fs arrival at the laboratory. . When the <br /> samples were shipped, the person in custody of them relinquished the <br /> samples by signing the chain-of-Custody form and noting the time. The <br /> sample-control officer at the laboratory verified sample integrity and <br /> confirmed that it was collected in the proper container, preserved <br /> correctly, and that there was an adequate volume for analysis. <br /> If these conditions were met, the sample was assigned a unique loc. <br /> number for identification throughout analysis and <br /> reporting. <br /> 5 <br /> yThe Yo <br /> number was recorded on the chain-of-custody form and in the legallyg <br /> I required log book maintained by the laboratory in the laboratory. The <br /> sample description, date received, client's name and any other <br /> relevant information was also recorded. <br /> 3.3 Ana tical Quality Asaurance <br /> l <br /> In addition to routine calibration of the analytical instruments with <br /> standards and blank, the analyst is required to run duplicates and <br /> ._ spikes-on--20--percent--of--the-analyses-to--insure - <br /> �. precision and accuracy. :Accuracy is also verified through the follow- <br /> ing. <br /> N _ <br />