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Sequoia 680 Chesapeake Dnve Redwood City,CA 94063 (415) 364 9600 FAX(415)364-9233 <br /> (D- Analytical 404 N Wigct Lane Walnut Creek CA 94596 (510) 988 9600 FAX(510)988-9673 <br /> 819 Sinker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 96M FAX(916)921-0100 <br /> L s v xr.ry <,n <br /> gro West, Inc A Cllernt Project)0 "Shell, 420 Mst Ketdeman Lane,Lodi, CA" v <br /> ` 1050 Melody Lane, Ste 160 Matrix Sall <br /> Roseville, CA 95678 <br /> Attention David L Poulsen QC Sample Group 508-0481 Reported Aug 21, 1995 <br /> C .. u .-4: k Ox;r ,. .... .. ,.,.,..,.�.. rw�An��Av4}3� v�>,.n xv N4tiKn �%r[�}}d�Op,✓..�frani,»w . h i,.w Cv ' v <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE <br /> Cadmium Chromium Lead Nickel Zinc Mercury <br /> Method EPA 6010 EPA 6010 EPA 6010 EPA 6010 EPA 6010 EPA 7471 <br /> Analyst: K Barta K Barta K Barta K Barta K Barta K Barta <br /> Concentration <br /> Spiked 50 mg/kg 50 mg/kg 50 mg/kg 5o mg/kg 50 mg/kg 0.25 mg/kg <br /> LCS Batch#- LCS081495 LCS081495 LCS081495 LCSW1495 LCS081495 LCS081795 <br /> Date Prepared- 8/14/95 8/14/95 8/14/95 8/14/95 8/14/95 8/17/95 <br /> Date Analyzed 8/18/95 8/18/95 8/18/95 8/18/95 8/18/95 8/19/95 <br /> Instrument I.D # P-40 P-40 P-40 P-40 P-40 SH-1000 <br /> LCS % <br /> Recovery 98 97 97 100 98 106 <br /> Control Limits. 8x120 80-120 80-120 80-120 80120 80-124 <br /> r �< ,,.4 r ,..,.Y v ., r,. ,r r x y.v..s..a.M x..r v.r ,., ,. ,V...�.,,.,.�,xr%,.sc,rw.' ,n...,..,,;,rcv�,9cr ,..G:twc.✓`.`„.r r�.'+v.�. N z`S ,r,t»:',.. v r.u}r, r w.. <br /> MS/MSD <br /> Batch# 5080481 5080481 5080481 5080481 5080481 5080504 <br /> Date Prepared: 8/14/95 8/14/95 8/14/95 8/14/95 8/14/95 8/17/95 <br /> Date Analyzed 8/18/95 8/18/95 8/18/95 8/18/95 8/18/95 8/19/95 <br /> Instrument l D.#. P-40 P-40 P-40 P-40 P-40 SH-1000 <br /> Matrix Spike <br /> % Recovery: 96 91 89 94 88 100 <br /> Matrix Spike <br /> Duplicate% <br /> Recovery: 96 93 94 92 92 104 <br /> Relative% <br /> Difference 0 0 22 54 2.2 44 3 9 <br /> Please Note <br /> The LCS is a control sample of known,interferent free matrix that Is analyzed using the same reagents, <br /> EO OIA ANALYTICAL preparation and analytical methods employed for the samples The LCS%recovery data is used for <br /> /7 validation of sample batch results Due to matrix effects,the QC limits for MS/MSG's are advisory only <br /> ��`.•�f„/,� and are not used to accept or reject batch results <br /> Linda C Schneider CGL <br /> Project Manager <br /> 5084481 FUG <4> <br />