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' SEQUOIA ANALYTICAL <br /> Y 11 <br /> 819 Striker Avenue, Suite 8 • Sacramento CA 95834 <br /> (916) 921-9600 • FAX (916) 921-0100 <br /> IO <br /> EMCON Assocsates h K Chant Project ID Shell, 420 W Ketdeman Ln, Lodi Sampled' v. Oct 5, 1992 <br /> 1433 N Market Blvd Sample Matrix Water Received Oct 6, 1992 <br /> Sacramento, CA 95$34 Analysis Method EPA 5030/8015/8020 Reported Oct 16, 1992 <br /> Attention Jim Pittilla First Sample# 210-0086 <br /> TOTAL PURGEABLE PETROLEUM HYDROCARBONS with BTEX DISTINCTION <br /> Reporting Sample Sample Sample Sample Sample <br /> Analyte Limit I.D. I.D. I.D. I D. I.D. <br /> ppm 210-0086 210-0087 210-0088 210-0089 210-0090 <br /> MW-1 MW-2 MW-3 Feld Blank Trip Bank <br /> urgea e <br /> Hydrocarbons 0 050 N D N D N D N D N D <br /> Benzene 000050 00013 N D N D N D N D <br /> Toluene 000050 N D N D N D N D N D <br /> Ethyl Benzene 000050 N D N D N D N D N D <br /> Total Xylenes 000050 N D N D N D N D N D <br /> Chromatogram Pattern Gas <br /> Quality Control Data <br /> Report Limit Multiplication Factor 10 1 0 10 10 1 0 <br /> Date Analyzed 10/13/92 10/13/92 10/13/92 10/13/92 10/13/92 <br /> Instrument Identlflcatlon HP-1 HP-1 HP-1 HP-1 HP-1 <br /> Surrogate Recovery, % 93 93 93 93 90 <br /> (OC Limits = 70-130%) <br /> Purgeable Hydrocarbons are Guanbtated against a fresh gasoline standard <br /> Analytes reported as N 0 were not detected above the stated reporting limit. <br /> SEQUOIA ANALYTICAL <br /> 0 <br /> Michael R Was <br /> Laboratory Director <br /> 2100086 EMC <1> <br />