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Date Alpha Analytical, Inc - a Work Order <br /> 16-Apr-01 p Y � IQC Summary Report P 03043260 <br /> Method Blank Test Code SW82608 Batch ID MS9S0329A Analysis Date 03/29/2001 12 09 <br /> Sample ID MBLK_01032869 Units pg/Kg Run ID Manual—01040920 Prep Date 03/2912001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> 0Methyl Cert-butyl ether(MTBE) ND 5 <br /> enzene ND 5 <br /> oluene ND 5 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Laboratory Control Spike Test Code SW0260B Batch ID MSSS0329A Analysis Date 031301200108 02 <br /> Sample ID LCS_01033006 Units jig/Kg Run ID Manual_01040920 Prep Date 03/30/2001 <br /> Analyte Result PQL SpkVal SpkReNal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Methyl tert-butyl ether(MTBE) 180 20 200 90 65 135 <br /> Benzene 191 20 200 96 65 135 <br /> Toluene 189 20 200 95 65 135 <br /> Ethylbenzene 177 20 200 88 65 135 <br /> m,p-Xylene 337 20 400 84 65 135 <br /> o-Xylene 165 20 200 82 65 135 <br /> Sample Matrix Spike Test Code SW0260B Batch ID MS9S0329A Analysts Date 03/30/2001 11 42 <br /> Sample ID 01032862-02AMS Units pg/Kg Run ID Manual_01040920 Prep Date 03/30/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLtmil HighLimit RPD Ref Val %RPD Qual <br /> Methyl tert-butyl ether(MTBE) 438 40 400 0 110 65 135 <br /> Benzene 388 40 400 0 97 65 135 <br /> Toluene 370 40 400 0 93 65 135 <br /> Ethylbenzene 337 40 400 0 84 65 135 <br /> m,p-Xylene 625 40 800 0 78 65 135 <br /> o-Xylene 316 40 400 0 79 65 135 <br /> Sample Matrix Spike Duplicate Test Code SW8260B Batch ID MS9S0329A Analysis Date 03/3012001 18 52 <br /> Sample ID 01032862-02AMSD Units pg/Kg Run ID Manual 01040920 Prep Date 03/30/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> ethyl tert-butyl ether(MTBE) 382 40 400 0 96 65 135 4381 136 <br /> enzene 374 40 400 0 94 65 135 3883 3 71 <br /> oluene 356 40 400 0 89 65 135 3705 403 <br /> Ethylbenzene 330 40 400 0 83 65 135 3374 2 17 <br /> m p-Xylene 627 40 800 0 78 65 135 6253 0 327 <br /> o-Xylene 315 40 400 0 79 65 135 316 0 292 <br /> Comments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matnx <br /> B-Analyte detected in the associated Method Blank <br /> s <br />