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THE <br /> REPORT DATE March 10, 2003 CLIENT: SHAW GROUP <br /> LABORATORY ID 703-0847.12 PAGE 26 of 70 <br /> TWINING DATE SAMPLED 02-18-03 at 1230 by Randy E. Kirby METHOD. EPA 8270 <br /> DATE RECEIVED : 02-21-03 at 1438 from Randy E. Kirby UNITS: mg/kg <br /> L A B 0 R A T 0 P I E S I N C DATE PREPARED 02-25-03 DATE ANALYZED'. 03-02-03 <br /> ANALYZED BY : C. Eammatre REVIEWED BY: J. Ureno <br /> CLIENT SAMPLE ID : PIPE-1 SAMPLE TYPE Soil <br /> CONSTITUENT RESULT DLR CONSTITUENT RESULT DLR CONSTITUENT RESULT DLR <br /> 1.0 <br /> Acenaphthene NO 1.0 2,4-Dichlorophenol ND 1.D N-Nitrosodi-n-propylamine ND <br /> 10 <br /> Acenaphthylene NO 1.0 2:6-Uichlorcphenol ND ,0 Pentarhicrophenol ND <br /> 1.0 <br /> Aniline NO 1.0 Diethylphthalate NO 1.0 Phenanthrene NO <br /> 10 <br /> Anthracene NO 1.0 Dlmethylphthalate NO 1.0 Phenol NO <br /> 10 <br /> Benzidine NO 1.0 2.4-Dimethylphenol NO 1.0 Pyrene NO <br /> 1 0 <br /> Benzoic Aad ND 1_b 2.4-Dinitrophenol ND 1,2.4-Tirrhlorobenzene ND <br /> 16 <br /> Benzo(a)anthracene NO 1.0 2.4-Dinitrotoluene ND 10 2,4,5-Tnrhloropherol NO <br /> 1G <br /> Benzo(a)pyrene NO 1.6 2.6-Oinitrotoluene NO 1.0 2,4,6-Trichlorophenol NO <br /> 10 <br /> Benzo(b)fluoranthene NO 1_C 1.2-Diphenylhydrazina(Azabenzene} ND 10 Aldrin NO <br /> 1n <br /> Benzo(g,h.i)perylene ND 1.0 Di-n-octylphthalate ND 1.0 a-BHC NO <br /> f4 <br /> Benzo(k)fluoranthene ND 1.0 Fluoranthene NO 1.0 b-BHC ND <br /> 1.6 <br /> Beni Alcohel NO 1 0 Fluorene ND 1.0 d-BHC ND <br /> 1.0 1 0 1.0 <br /> pis(2�hloroelhi methane NQ Hexachlorobenzene INDg-DHC(Llndane) NO <br /> 1.0 <br /> Bis(2-chloroethyl)ether NO 1.0 Hexachlorobutadine ND 1 0 DOD ND <br /> 1.0 <br /> Bis(2-cHoroisopropyq ether NO to <br /> Hexachlorocyclopentadiene ND 1 0 DDE NO <br /> 4,4 <br /> Bis(2-ethylhexyl}phthalate NO 1.0 Hexachloroethane ND 1 0 DDT ND <br /> 1a <br /> 4-Bromophenyl phenyl ether ND 10 <br /> lndeno{1,2,3cd)Pyrene ND 1.0 Dieldrin NO <br /> 10 <br /> Butyl benzyl phthalate ND 1.0 lsophorone ND 1.0 Endosultan 1 ND <br /> 1.0 <br /> 4-Chloroaniline ND 1.0 2-Methyl-4,13tiinitrophenol ND 1,0 Endosultan ll NO <br /> M14 <br /> 2-Chloronaphthaiene NO 1,0 2-Methylnaphthalene NO 1,0 Endosultari Sulfate ND <br /> 1.0 <br /> 4-Chloro3-methylphenol ND 10 <br /> 2-Methylphenol(0-cresol) NO 1'0 Endrin NO <br /> 14 <br /> 2-Chlorophenol ND 1.0 4-rnethylphenol(ptsesol) ND 1.6 Endrin Aldei ND <br /> 16 <br /> 4-Chlorophenyl phenyl ether ND 1.0 Naphthalene ND 1.0 Heptachlor ND <br /> 1.0 <br /> Chrysene ND 10 <br /> 2-Nitroaniline NO 1 0 Heptachlor epoxide ND <br /> Dibenza{a,h)Anthracene ND 10 <br /> 3-Nitroaniline NO 0 SURROGATE RECOVERY RANGE <br /> Dibenzofuran ND 10 <br /> 4-Ni1roaniline NO 1.0 2-Fluorphenoi 21.6 21-160% <br /> Dim-butylphthalate ND 1.0 Nitrobenzene NO 10 Phenoi-d6 30.5 10-94% <br /> 1.3-Dichloroben7ene ND 1.0 2-Nitrophenol ND 1.0 Nitrobenzene-d5 58.8 35-114% <br /> 1,4-Dichlorobenzene NO 1.0 4-Nitrophenolp y <br /> ND 1. 2-Fluoro hen I 52'1 43-116% <br /> 12-Cich0robenzene NO 10 N-Nitrosodimethylamine ND 1.0 2,4.6-Tribromophenol 102 10-123/ <br /> 3,3'-Dichlarobenzidine ND 1.0 N-N(trosodiphenylamine NO 1.0 D14-Tarphenyl 07.1 70-1301A <br /> rLR:Detection Limit for Reporting Purposes mg/kg:Milligrams per kilogram(ppm) ND'.None Detected <br />