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S ECO R - <br /> ATTACHMENT G <br /> FIELD AND LABORATORY PROCEDURES <br /> Soil Borings and Sampling <br /> The soil borings will be drilled using a 4-inch hand auger to depths of approximately 10 feet bgs. The <br /> sampler will be driven a maximum of 18 inches using a slide sampler. Soil samples collected for <br /> chemical analysis will be retained in brass liners, capped with Teflon squares and plastic end caps, <br /> and sealed in clean zip-lock bags. The samples will be placed on ice for transport to the laboratory <br /> accompanied by chain-of-custody record. Down-hole augering and sampling equipment will be <br /> steam-cleaned prior to and following completion of each sample interval. <br /> Temporary Well Installation and Sampling <br /> The borings will be converted to temporary groundwater monitoring wells by installing 2-inch <br /> diameter, flush-threaded, Schedule 40 PVC casing with 0.020-inch factory-slotted screen. Approxi- <br /> mately 10 foot of screen will be placed in the bottom of each boring and threaded to a solid well k <br /> casing section will extend above the ground surface approximately one foot. <br /> Groundwater samples will be collected using dedicated polyethylene tubing and a peristaltic pump, <br /> placed into appropriate EPA-approved containers, labeled, placed on ice, and transported to a <br /> California State Certified laboratory accompanied by chain-of-custody documentation. Water Quality <br /> measurements including conductivity, turbidity, temperature and PH will be collected during well <br /> sampling activities. <br /> Organic Vapor Monitoring Procedures <br /> Soil samples collected at 5-foot depth intervals during hand augering and will be analyzed in the field <br /> for ionizable organic compounds using a photo-ionization detector (PID) with a 10.2 UV lamp or a <br /> flame ionization detector (FID). The test procedure will involve measuring approximately 30 grams <br /> from an undisturbed soil sample, placing this subsample in a sealed container (either a zip-lock bag <br /> or a mason jar). The container will be warmed for approximately 20 minutes (in the sun), then the <br /> head-space within will be tested for total organic vapor, measured in parts per million as benzene <br /> (ppm; volume/volume). The instrument will be calibrated prior to drilling using a 100-ppm isobutylene <br /> standard (in air) and a sensitivity factor of 55, which relates the photo-ionization potential of benzene <br /> to that of isobutylene at 100 ppm. PID and FID readings are useful for indicating relative levels of <br /> contamination, but cannot be used to evaluate hydrocarbon levels with the confidence of laboratory <br /> analyses. <br /> Laboratory Procedures for Soil and Ground water Samples <br /> Selected soil and water samples collected will be analyzed for the presence of TPHg and TPHd by <br /> EPA Method 8015, BTEX and fuel oxygenates MtBE, EtBE, TBA, TAME, DIPE, EDB, and 1,2-DCA <br /> by EPA 8260 and total lead by EPA Method 7421. <br /> Soil Cuttings and Rinsate Water <br /> Soil cuttings generated during drilling operations will be temporarily stored on site and covered with <br /> plastic sheeting pending characterization and disposal. Soil cuttings will be removed by Chevron's <br /> disposal contractor to an appropriate disposal facility. Water generated during steam cleaning will be <br /> temporarily stored in DOT-approved 55-gallon drums pending transport by Chevron's disposal <br /> contractor to an appropriate disposal or treatment facility. Soil cuttings and rinsate water drums will <br /> be temporarily stored on site for approximately 4 to 8 weeks. <br />