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110 2nd Avenue South,#ED7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc. Telephone�925a9e-1620 Fax:925-798-1622 <br /> http:!/www.mccampbell.com E-mail:main(a]mccampbell.com <br /> Advanced GeoEnvironmental, Inc Client Project ID: Van Buskirk Date Sampled: 09/24/02 <br /> 837 Shaw Road Date Received: 09/25/02 <br /> tStockton,CA 95215 Client Contact: Bili Little Date Extracted: 09/27/02-10/01/02 <br /> Client P.O.: Date Analyzed: 09127/02-10101/02 <br /> ' Oxygenates and BTEX by GCIMS* <br /> Extraction Method:-SW5030B Analytical Method:SW8260B Work Order.0209390 <br /> ' Lab ID 0209390-OOIB ! 0209390-002B 0209390-003B { 0209390-004B <br /> Client ID MW3/092402 j MW4/092402 MWS/092402 MW6/092402 <br /> Reporting Limit for <br /> ' Matrix W ---- '-- W � W---------- --- W__— DF=1 <br /> DF 1 10 1 5 s w <br /> tCompound Concentration ug/kg µg/1.. <br /> tert-Amyl methyl ether(TAME) ND ND<5.0 ND ND<2.5 NA 0.5 <br /> Benzene ND ND<5.0 ND NI3<2.5 NA 0.5 <br /> t-Butyl alcohol(TBA) ND NIX50 ND ` ND<25 NA 5.0 <br /> Diisopro 1 ether(DiPE ND ND<5.0 ND ND<2.5 <br /> PY ) NA 0.5 <br /> Ethylbenzene ND ND<5.0 ND ND<2.5 NA 0.5 <br /> Ethyl tert-butyl ether(ETBE) ND ND<5.0 ND I ND<2.5 NA 0.5 <br /> Methyl-t-butyl ether(MTB)F} 1.0 290 ND i 120 NA 0.5 <br /> Toluene 0.78 ND<5.0 ND ND<2.5 NA 0.5 <br /> Xylenes ND ND<5.0 ND ND<2.5 NA 0.5 <br /> ' Surrogate Recoveries (%) <br /> %3S: 98.9 105 105 99.4 <br /> Comments i I <br /> R <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in uglL,soil/sludge/solid samples in ug/kg, wipe samples in ug(wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> h)lighter than water immiscible sheen/product is present; i}liquid sample that contains greater than—2 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> } <br /> • <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />