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h IWO_ M i = M T T a M M M Roy F. Weston, Inc. Stockton Laboratory Semivolatiles by GC/MS, HSL List Report Date: 12/11/91 10.25 RFW Batch Number. 91125471 Client: TREATEK Work Order: 2391-16-06-000_ _ _Pam Cust ID: MIL GRENE SBLK SBLK BS SBLK BSD SPI Sample RFW#. 001 91SE0415-MB2 91SE0415-MB2 91SE0415-MB2 Information Matrix: SOIL SOIL SOIL SOIL Q.F. : 1.00 2.00 1 .00 1.00 Units: ug/Kg ug/Kg ug/Kg ug/Kg Nitrobenzene-d5 82 % 81 % 82 % 95 % Surrogate 2-Fluorobiphenyl 93 % 86 % 89 % 100 % Recovery p-Terphenyl -d14 76 % 88 % 92 % 98 % Phenol -d5 79 % 75 % 74 % 84 % 2-Fluorophenol 75 % 77 % 82 % 89 % 2,4,6-Br3-phenol 117 % 121 % 126 * % 146 * % Phenol 380 U 670 U 56 % 68 % bis(2-Chloroethyl)ether 380 U 670 U 330 U 330 U 2-Chlorophenol 380 U 670 U 59 % 67 % 1,3-Dichlorobenzene 380 U 670 U 330 U 330 U 1,4-Dichlorobenzene 380 U 670 U 64 % 75 % Benzyl alcohol 380 U 670 U 330 U 330 U 1,2-Dichlorobenzene 380 U 670 U 330 U 330 U 2-Methylphenol 380 U 670 U 330 U 330 U bis(2-Chloroisopropyl )ether 380 U 670 U 330 U 330 U 4-Methylphenol 380 U 670 U 330 U 330 U N-Nitroso-Di-n-propylamine 380 U 670 U 76 % 89 % Hexachloroethane 380 U 670 U 330 U 330 U Nitrobenzene 380 U 670 U 330 U 330 U Isophorone 380 U 670 U 330 U 330 U 2-Nitrophenol 380 U 670 U 330 U 330 U 2,4-Dimethylphenol 380 U 670 U 330 U 330 U Benzoic acid 1900 U 3300 U 1700 U 1700 U bis(2-Chloroethoxy)methane 380 U 670 U 330 U 330 U 2,4-Dichlorophenol 380 U 670 U 330 U 330 U 1,2,4-Trichlorobenzene 380 U 670 U 67 % 78 % Naphthalene 380 U 670 U 330 U 330 U 4-Chloroaniline 380 U 670 U 330 U 330 U Hexachlorobutadiene 380 U 670 U 330 U 330 U 4-Chloro-3-methylphenol 380 U 670 U 58 % 73 % 2-Methylnaphthalene 380 U 670 U 330 U 330 U Hexachlorocyclopentadiene 380 U 670 U 330 U 330 U *= Outside of EPA CLP QC limits