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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-I620 Fax 925-798-1622 <br /> Ihttti//www mccampbell corn E-mail main@mccampbell corn <br /> i <br /> Advanced GeoEnvironmental Client Project ID Flame Liquors Date Sampled 03/10/2002 <br /> 837 Shaw Road Date Received 03/12/2002 <br /> IStockton, CA 95215 Client Contact Calvin Lee Date Extracted 03/13-03115/2002 <br /> Client P O Date Analyzed 03113-03/1512002 <br /> IGasoline Range(C&C12)Volatile Hydrocarbons as Gasolene*,with Methyl tert-Butyl Ether* & BTEX* <br /> EPA methods 5030,modified 8015,and 8020 or 602,California RWQCB(SF Bay Region)method GCFID(5030) <br /> Lab ID Client ID Matrix TPH(g)+ MTBE Benzene Toluene Ethyl- Xylenes %Recovery <br /> benzene Surrogate <br /> -001 0331001002 <br /> 02-3200 W ND ND ND ND ND ND 102 <br /> I 0203200 MW2/ W 800,a 1I,000 39 ND<5 0 45 79 106 <br /> -002 031002 <br /> 0203200 MW3/ W 61,a 34 060 ND ND ND 103 <br /> -003 031002 <br /> I <br /> I <br />' Reporting Limit unless W 50 ug/L 50 05 05 05 05 <br /> otherwise stated,ND <br /> means not detected above <br /> the reporting limit S 1 0 mg/kg 005 0 005 0 005 0 005 0 005 <br />' <br /> *water and vapor samples are reported in ug/L,wipe samples to ug/wipe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ug/L <br />' cluttered chromatogram,sample peak coelutes with surrogate peak <br /> `The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a) unmodified or weakly modified gasoline is significant b) heavier gasoline range compounds are significant(aged <br />' gasoline?), c) lighter gasoline range compounds (the most mobile fraction) are significant, d) gasoline range compounds having broad <br /> chromatographic peaks are significant,biologically altered gasohne9,e)TPM pattern that does not appear to be derived from gasoline(9),f) <br /> one to a few isolated peaks present,g)strongly aged gasoline or diesel range compounds are significant,h)lighter than water immiscible <br /> sheen is present i)liquid sample that contains greater than—5 vol %sediment,j)no recognizable pattern <br />' DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />