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1 <br /> 110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br />' MCCAMPBELL ANALYTICAL INC. Telephone 925-798-1620 Fax 925-798-1622 <br /> //www mccamnbell comcom E-mail matn@mccampbell corn <br /> i <br /> Advanced GeoEnvironmental Client Project ID Flame Liquor Date Sampled 09/23/99 <br /> 4005 North Wilson Way Date Received 09/25/99 <br /> Stockton, CA 95205 Client Contact Tony Mikacich Date Extracted 09/28/99 <br />' <br /> [Client P O Date Analyzed 09/28-09/30/99 <br /> Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br />' Lab ID 22148 22150 22152 22154 <br /> Reporting Luna <br /> Client ID P1-35' Pi-45' Pi-55' P1-W <br />' Matrix S S S W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND ND ND ND<10 50 1 0 <br />' Ethyl tert-Butyl Ether(ErBE) ND ND ND ND<10 50 10 <br /> lie Methyl-tert Butyl Ether(MTBE) 28 9 1 16 420 50 10 <br /> tent-Amyl Methyl Ether(TAME) ND ND ND ND<10 50 10 <br />' tert-Butanol ND ND ND ND<50 25 50 <br />' Surrogate Recoveries(%) <br />' Dibromofluoromethane 98 95 92 97 <br /> Comments <br />' 'waterles are reported to u <br /> camp p g/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC!SPLP extracts to ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br />' (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 / Edward Hartulton,Lab Director <br />