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1 <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccarripbell corn E-mail matn@mccatnpbell corn <br /> Advanced GeoEnvtronmental Client Project ID Flame Liquor Date Sampled 11/04-11/05/99 <br /> 4005 North Wilson Way Date Received 11/09/99 <br /> Stockton, CA 95205 Client Contact Tony Mikacich Date Extracted 11/12-11/16/99 <br />' Client P O Date Analyzed 11/12-11/16/99 <br /> Oxygenated Volatde Organa cs By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 25142 25158 25162 25177 <br /> Reporting Limit <br /> Client ID MW-1-W MW-2-W MW-3-W MW-4-W <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND ND<5 ND<2 5 ND 50 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND<5 ND<2 5 ND 50 10 <br /> Methyl-tent Butyl Ether(MTBE) 40 95 73 ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND<5 ND<2 5 ND 50 10 <br /> tert-Butanol ND ND<25 ND<13 ND 25 5 0 <br /> Surrogate Recoveries(%) <br /> IDibromofluoromethane 93 91 97 86 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> IDHS Certification No 1644 I _Edward Hamilton,Lab Director <br /> I <br />