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1 <br /> 1 <br /> . CASTLE ANALYTICAL LABORATORY <br />' Environmental Testing Services 2333 Shuttle Drive Atwater CA 95301 Phone (209)384-2930 <br /> Fax (209)384-1507 <br />' Advanced GecEnvlronmental, Inc Client Project ID Flame Mini Mart Method EPA 5030/8260 <br /> of Northern California Reference Number 5916 Instrument ID HP Series 11 <br /> 837 Shaw Road Matrix Soil Prepared 07-25-03 <br /> Stockton CA 95215 Analyst S Foster Analyzed 07-26-03 <br />' Attn Tim Cuellar Reported 07-30-03 <br /> QUALITY CONTROL DATA REPORT <br />' SPIKE ID VSMS-7253 <br />' Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> mg/Kg mg/Kg m IK %R <br /> COMPOUNDS <br />' t-But I Alcohol(t-BA) 080 ND 300 110% 70-130 <br /> Methyl t-but I ether (MTBE) 0 010 ND 0 100 872% 70-130 <br /> Ditso ro I ether(DIPS) 0 010 ND 0 100 796% 70-130 <br /> Ethyl t-But l ether(ETBE) 0 010 ND 0 100 900% 70-130 <br />' t-Am I Methyl ether(TAME) 0 010 ND 0 100 868% 70-130 <br /> 1 2-Dichloroethane(1 2-DCA) 0 010 ND 0 100 128% 70-130 <br /> Ethylene dibromide(EDB) 0 010 NO 0 100 928% 70-130 <br /> Surrogates <br /> 1 <br /> 1 2-Dichloroethane-d4 0 010 108% 0 400 125% 70-130 <br /> Toluene-d8 0 010 105% 0 400 100% 70-130 <br />' Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> m lK %R %R <br /> COMPOUNDS <br />' t-But €Alcohol ft-BA) 300 876% 849% 70-130 290% <br /> Methyl t-but i ether (MTBE) 0 100 692% 109% 70-130 410% <br /> Diisoprop I ether(DIPE) 0 100 656% 112% 70-130 505% <br /> Ethyl t-But I ether(ETBE) 0 100 940% 121% 70-130 250% <br />' t-Amyl methyl ether(TAME) 0 100 624% 764% 70-130 169% <br /> 1 2-Dichloroethane(1 2-DCA) 0 100 996% 924% 70-130 750% <br /> Ethylene dibromide(EDB) 0 100 i 816% 876% 70-130 709% <br /> Surrogate <br />' 1 2-Dichloroethane-d4 0 400 886% 963% 70-130 833% <br /> Toluene-d8 0 400 924% 96 0% 70-130 382% <br /> I <br />' The LCS (Laboratory Check Sample) is a control sample of known, Interferent free matrix that is fortified with representative analytes and <br /> analyzed using the same reagents, preparation and analytical methods employed for the samples The LCS %recovery is used for validation <br /> of sample batch results Due to matrix effects the OC limits and recoveries for MSIMSD's are advisory only and are not used to accept or <br /> reject batch results <br /> ANALYST L/ � APPROVED 13Y <br /> Clan J Cane Ja,shes Phillips <br /> Iboratory Director <br />