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' CASTLE ANALYTICAL LABORATORY <br />' Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209)384-2930 <br /> Certificate No 2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental, Inc Client Project ID Flame Mini Mart Sampled 07-24-03 <br />' of Northern California Reference Number 5922 Received 07-25-03 <br /> 837 Shaw Road Sample Description Water Extracted 07-25-03 <br /> Stockton CA 95215 Sample Prep/Analysis Method EPA 5030!8260 Analyzed 07-25-03 <br /> Attn Tim Cuellar Lab Numbers 5922-1W 2W Reported 08-08-03 <br />' GASOLINE ADDITIVES AND SOLVENTS BY FPA METHOD 8260 GC/MS <br /> ANALYTE REPORTING SAMPLE ID SAMPLE ID <br />' LIMIT MW 6 MW 7 <br /> 072403 072403 <br /> I FLIEL OXYGE ATES <br /> Methyl tert-Butyl Ether(MTBE) 050 11 160 <br /> Di-isopropyl Ether (DIPE) 050 ND ND <br /> Ethyl tert-Butyl Ether (ETBE) 050 NO NO <br /> tert-Amyl Methyl Ether(TAME) 050 NO 13 <br /> tert-Butanol(TBA) 20 NO NO <br /> VOLATILE HALOCARBD S <br /> 1 2-D3chloroethane (1,2-OCA) 050 NO ND <br /> IEthylene Dibromide (EDB) 050 ND NO <br /> Report Limit Multiplication Factor 1 1 <br /> Report Lima Multiplication Factor for MTBE 10 <br /> Surrogate Recoveries <br /> 1 2-Dichloroethane-d4 944% 969% <br /> Toluene-d8 102% 103% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> (pg/L)= micrograms per liter or panrbill (ppb) <br /> ANALYST AA APPROVED BY <br /> 91"'A <br /> Clan Cone J Phr!lrps <br /> aboratory Director <br />