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I <br /> I <br /> CASTLE ANALYTICAL LABORATORY <br />' Environmental Testing Services 2333 Shuttle Dnve,Atwater CA 95301 Phone (209)384-2930 <br /> Certificate No 2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental Inc Client Project ID Flame(Liquors)Mini Mart Sampled 09-22-03 <br />' of Northern Caloforma Reference Number 6121 Received 09-23-03 <br /> 837 Shaw Road Sample Description Water Extracted 09-28-03 <br /> Stockton CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 09-28-03 <br /> Attn Tire Cuellar Lab Numbers 6121-6W Reported 10-01-03 <br />' GASOLINE ADDITIVES AND SOLVENTS BY EPA METHOD 8260 GC/MS <br /> ANALYTE REPORTING SAMPLE ID <br />' LIMIT MW 7 <br /> 092203 <br /> IL) (u IL) <br />' FUEL OXYGENATES <br /> Methyl tert-Butyl Ether(MTBE) 050 16 <br /> Di-+sopropyl Ether (DIPE) 050 ND <br /> Ethyl tert-Butyl Ether (ETRE) 050 ND <br /> tert-Amyl Methyl Ether(TAME) 050 ND <br /> Cert-Butanol(TBA) 20 ND <br />' VOLATILE HALOCARSONS <br /> 1 2-Dichlorcethane (1 2-DCA) 050 ND <br />' Ethylene Dibromide (EDB) 050 ND <br /> Report Limit Multiplication Factor 1 <br /> Surrogate Recoveries <br />' 1 2-Dichloroethane-d4 928% <br /> Toluene-d8 975% <br /> Instrument iD HP 5972 MS <br /> I Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitatson Limit=Reporting Limit x Report Limit Multiplication Factor <br /> (pg/L)= micrograms per liter or arts per billion(ppb) <br /> ANALYST APPROVED BY <br /> Cfarr J Gone Jam '11, S <br /> La ratory Director <br />