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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209) 572-0916 <br /> Report# R201-07 CERTIFICATE OF ANALYSIS Date: 7/22/05 <br /> ,.M. d <br /> J. KloberDate Rec'd: 7/20/05 <br /> anz &Associates Date Started: 7/21/05 <br /> P.Q.Box 576981 Project: Pombo Ranch Quarterly Date Completed:7/21/05 <br /> Modesto CA 95357 <br /> Date Sampled: 7/20/05 <br /> PO# Time: <br /> Sample ID: MW-105 Sampler <br /> Lab ID: 8304690 <br /> Method RL Analyte Results Units <br /> 82608 0.3 Benzene ND ug/L <br /> 0.3 Toluene ND <br /> 0.3 Ethyl Benzene ND <br /> 0.6 Total Xylenes ND <br /> 0.5 Methyl tert-butyl ether(MTBE) ND <br /> 40 Ethanol ND <br /> 5 tert-Butanol ND <br /> 0.5 di-Isopropyl ether(D1PE) ND <br /> 0.5 Ethyl tert-butyl ether(ETRE) ND <br /> 0.5 tert-Amyl methyl ether(TAME) ND <br /> 1.0 Ethylene dibromide(EDB) ND <br /> 0.5 1,2-Dichloroethane(1,2-DCA) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit°10 <br /> 1,2-Dichloroethane-d4 5.00 5.17 103.4 72-132 <br /> 2-Bromo-l-chloropropane 5.00 4.62 92.4 71-134 <br /> 4-Bromofluorobenzene 5.00 5.37 107.4 74-132 <br /> Robert Sereno Donna Keller <br /> Chemist Certification # 2585 Laboratory Director <br />