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Entech Analytical Labs, Inc , Santa Clara, CA <br />' Lab Report No H3012007 Date 01/31/2003 Page 9 <br /> 4 <br /> Project Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-5 Lab Samp ID 32975-006 <br /> Descr/Location MW-5 Recd Date 01/22/2003 <br /> Sample Date 09/17/2003 Prep Date 01/23/2003 <br />' Sample Time 1326 Analysis Date 01/23/2003 <br /> Matrix Water QC Batch WMS11896 <br /> Basis Not Filtered Notes <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dd <br /> Methyl-tert-butyl ether(MTBE) 03 1 PQL NO UG/L 1 <br />' Ethyl tert-butyl ether(ETRE) 05 5 PQL NO UG/L 1 <br /> tert-Amyl methyl ether(TAME) 03 5 PQL NO UG/L 1 <br /> Di-isopropyl ether(DIPS) 05 5 PQL NO UG/L 1 <br />' tert-Butyl alcohol (TBA) 46 10 PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromoffuorobenzene 65.135 SMEA 109% 1 <br /> Toluene-d8 77-150 SMEA 119% f 1 <br /> Dibromofluoromethane 57-156 SMEA 133% ; 1 <br /> I� <br /> I <br /> Approved by Date <br />