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Castle Analytical Laboratory, Atwater, CA <br />' Lab Report No H4062109 Date 06/30/2004 Page 2 <br />' Protect Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-10 Lab Samp ID 7085-10W <br /> Descr/Location MW-10 Rec'd Date 06/22/2004 <br />' Sample Date 06/18/2004 Prep Date 06/27/2004 <br /> Sample Time 1044 Analysis Date 06/27/2004 <br /> Matrix Water QC Batch VWMS-6274 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Di! <br /> Methyl-tert-butyl ether(MTBE) 0 289 05 MRL ND UG/L 1 <br /> Ethyl tert-butyl ether(ETRE) 0 084 05 MRL ND UG/L 1 <br /> tent-Amyl methyl ether(TAME) 0 067 05 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPS) 0155 05 MRL ND UG/L 1 <br />' tert-Butyl alcohol (TBA) 879 20 MRL ND UG/L 1 <br /> 1,2-Dichloroethane 0 081 05 MRL ND UG/L 1 <br /> 1,2-Dibromoethane 0 092 05 MRL ND UG/L 1 <br />' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 63-132 SLSA 938% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 840% 1 <br /> 1 <br />' Approved by _.__ Date 11), 0( <br /> i ' <br />