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' Castle Analytical Laboratory, Atwater, CA <br />' Lab Report No H4032509 Date 04/05/2004 Page 1 <br /> Project Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Project No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-1 Lab Samp ID 6796-1W <br /> Descr/Location MW 1 Recd Date 03/25/2004 <br /> Sample Date 03/24/2004 Prep Date 04/01/2004 <br />' Sample Time 1516 Analysis Date 04/01/2004 <br /> Matnx Water QC Batch VWMS-4014 <br /> Basis Not Filtered Notes DF <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dd <br /> Methyl-tart-butyl ether(MTBE) 289 50 MRL 130Q UGIL 100 <br /> Ethyl tert-butyl ether(ETBE) 0 840 5 MRL ND UG/L 10 <br />' tert-Amyl methyl ether(TAME) 0 670 5 MRL ND UG/L 10 <br /> Di-isopropyl ether(DIPE) 155 5 MRL ND UG/L 10 <br /> tert-Butyl alcohol (TBA) 879 200 MRL ND UG/L 10 <br />' 1,2-Dichloroethane 0 810 5 MRL ND UG/L 10 <br /> 1,2-Dibromoethane 0 920 5 MRL ND UG/L 10 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br />' Toluene-d8 76-129 SI_SA 955% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 978% 1 <br /> DF Reporting limits elevated due to matrix interferences <br /> 1 <br /> 1 <br /> 1A/,Approved by Date `7 <br /> 1 <br />