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' Castle Analytical Laboratory, Atwater, CA <br />' Lab Report No H4032509 Date 04/05/2004 Page 12 <br /> Project Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-3R Lab Samp ID 6796-3W <br /> Descr/Location MW-3R Rec'd Date 03/25/2004 <br /> Sample Date 03/24/2004 Prep Date 04/01/2004 <br />' Sample Time 1855 Analysis Date 04/01/2004 <br /> Matrix Water OC Batch VWMS-4014 <br /> Basis Not Filtered Notes DF <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl4ert-butyl ether(MTBE) 145 2.5 MRI` 9fi UG/L 5 <br /> Ethyl Cert-butyl ether(ETBE) 0420 2.5 MRL ND UG/L 5 <br />' tert-Amyl methyl ether(TAME) 0 335 2.5 MRL ND UG/L 5 <br /> Di-isopropyl ether(DIPE) 0 775 2.5 MRL ND UG/L 5 <br /> tert-Butyl alcohol (TBA) 440 100 MRL ND UG/L 5 <br />' 1,2-D{chloroethane 0405 2.5 MRL ND UGIL 5 <br /> 1,2-Dibromoethane 0460 25 MRL ND UG/L 5 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br />' Toluene-d8 76-129 SLSA 925% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 949% 1 <br />' DF Reporting limits elevated due to matrix interferences <br /> I <br /> 1 <br /> I <br /> Approved by Date <br />