ARCHIVED REPORTS_QUARTERLY MONITORING REPORT FIRST QUARTER 2007

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�r r ■r mom r Report Number: 54688 QC Report : Method Blank Data Date : 02/12/2007 Project Name : Unocal Op Unit Project Number : 6324.02 Method Method Measured Reporting Analysis Date Measured Reporting Analysis Date Parameter Value Limit Units Method Analyzed Parameter Value Limit Units Method Analyzed TPH as Diesel <50 50 ug/L M EPA 8015 02/06/2007 Benzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 TPH as Motor Oil <50 50 ug/L M EPA 8015 02/06/2007 Trichloroethene <0.50 0.50 ug/L EPA 8260B 02/07/2007 Octacosane(Diesel Surrogate) 95.0 % M EPA 8015 02/06/2007 1,2-Dichloropropane <0.50 0.50 ug/L EPA 8260B 02/07/2007 Bromodichloromethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 TPH as Diesel <50 50 ug/L M EPA 8015 02/12/2007 Dibromomethane <0.50 0.50 ug/L EPA 82608 02/07/2007 9 TPH as Motor Oil <50 50 ug/L M EPA 8015 02/12/2007 cis-1,3-Dichloropropene <0.50 0.50 ug/L EPA 8260B 02/07/2007 Octacosane(Diesel Surrogate) 96.0 % M EPA 8015 02/1212007 Toluene <0.50 0.50 ug/L EPA 82606 02/07/2007 trans-1,3-Dichloropropene <0.50 0.50 ug/L EPA 8260B 02/07/2007 9 TPH as Gasoline <50 50 ug/L EPA 8260B 02/07/2007 1,1,2-Trichloroethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,3-Dichloropropane <0.50 0.50 ug/L EPA 82608 02/07/2007 Methyl-t-butyl ether(MTBE) <0.50 0.50 ug/L EPA 8260B 02/07/2007 Tetrachloroethene <0.50 0.50 ug/L EPA 8260B 02/07/2007 Diisopropyl ether(DIPE) <0.50 0.50 ug/L EPA 8260B 02/07/2007 Dibromochloromethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 Ethyl-t-butyl ether(ETBE) <0.50 0.50 ug/L EPA 8260B 02/0712007 1,2-Dibromoethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 Tert-amyl methyl ether(TAME) <0.50 0.50 ug/L EPA 8260B 02/07/2007 Chlorobenzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 Tert-Butanol <5.0 5.0 ug/L EPA 8260B 02/07/2007 1,1,1,2-Tetrachloroethane <0.50 0.50 ug/L EPA 82608 02/07/2007 Methanol <50 so ug/L EPA 8260B 02/07/2007 Ethylbenzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 Ethanol <5.0 5.0 ug/L EPA 8260B 02/07/2007 P,M-Xylene <1.0 1.0 ug/L EPA 82608 02/07/2007 Dichlorodifluoromethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 O-Xylene <0.50 0.50 ug/L EPA 8260B 02/07/2007 Chloromethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 Styrene <0.50 0.50 ug/L EPA 8260B 02107/2007 Vinyl Chloride <0.50 0.50 ug/L EPA 8260B 02/07/2007 Isopropyl benzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 Bromomethane <20 20 ug/L EPA 82608 02/07/2007 Bromoform <0.50 0.50 ug/L EPA 8260B 02/07/2007 Chloroethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,1,2,2-Tetrachloroethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 Trichlorofluoromethane <0.50 0.50 ug/L EPA 82608 02/07/2007 1,2,3-Trichloropropane <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,1-Dichloroethene <0.50 0.50 ug/L EPA 8260B 02/07/2007 n-Propylbenzene <0.50 0.50 ug/L EPA 82608 02/07/2007 Methylene Chloride <5.0 5.0 ug/L EPA 8260B 02/07/2007 Bromobenzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 trans-1,2-Dichloroethene <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,3,5-Trimethylbenzene <0.50 0.50 ug/L EPA 82608 02/07/2007 1,1-Dichloroethane <0.50 0.50 ug/L EPA 82608 02/07/2007 2+4-Chlorotoluene <1.0 1.0 ug/L EPA 8260B 02/07/2007 2,2-Dichloropropane <0.50 0.50 ug/L EPA 8260B 02/07/2007 tert-Butylbenzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 cis-1,2-Dichloroethene <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,2,4-Trimethylbenzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 Chloroform <0.50 0.50 ug/L EPA 8260B 02/07/2007 sec-Butylbenzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 Bromochloromethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 p-Isopropyltoluene <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,11-Trichloroethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,3-Dichlorobenzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,1-Dichloropropene <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,4-Dichlorobenzene <0.50 0.50 ug/L EPA 82606 02/07/2007 1,2-Dichloroethane <0.50 0.50 ug/L EPA 8260B 02/07/2007 n-Butylbenzene <0.50 0.50 ug/L EPA 82608 02/07/2007 Carbon Tetrachloride <0.50 0.50 ug/L EPA 8260B 02/07/2007 1,2-Dichlorobenzene <0.50 0.50 ug/L EPA 8260B 02/07/2007 I�a.. Approved By. Jo�I;Kiff KIFF ANALYTICAL, LLC U2795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800