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CLIENT: McCampbell Analytical QC SUMMARY REPORT Work Order: 0008530 Project: 21611/Home Depot. Tracy Laboratory Control Spike Sample ID LCS-2628 Batch ID: 2628 Test Code: 8150S Units: pg/g Analysis Date 9/5/00 7:21:17 PM Prep Date 9/2/00 Client ID: Run ID: ORGC4_000905A SegNo: 107926 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Dalapon 4.024 1.0 5.00 0 80.5% 32 103 0 Dicamba 0.8567 0.20 1.00 0 85.7% 45 101 0 MCPP 385.7 100 500 0 77.1% 50 101 0 MCPA 408.9 100 500 0 81.8% 38 106 0 Dichlorprop 4.199 1.0 5.00 0 84.0% 42 108 0 2,4-D 4.296 1.0 5.00 0 85.9% 40 109 0 2,4,5-TP 0.4253 0.10 0.500 0 85.1% 42 105 0 2,4,5-T 0.4226 0.10 0.500 0 84.5% 36 105 0 2,4-DB 4.414 1.0 5.00 0 88.3% 44 110 0 Dinoseb 0.7769 0.20 1.00 0 77.7% 29 102 0 2,3-D 4.12 0.10 5.00 0 82.3% 35 119 0 Sample ID LCSD-2628 Batch ID 2628 Test Code: 8150S Units: pg/g Analysis Date 9/5/00 7:45:29 PM Prep Date 9/2/00 Client ID: Run ID: ORGC4_000905A SegNo: 107927 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Dalapon 3.816 1.0 5.00 0 76.3% 32 103 4.02 5.30% 37 Dicamba 0.8215 0.20 1.00 0 82.1% 45 101 0.857 4.20% 34 MCPP 366.2 100 500 0 73.2% 50 101 386 5.20% 46 MCPA 397.4 100 500 0 79.5% 38 106 409 2.85% 33 Dichlorprop 4.088 1.0 5.00 0 81.8% 42 108 4.20 2.66% 27 2,4-D 4.128 1.0 5.00 0 82.6% 40 109 4.30 3.98% 28 2,4,5-TP 0.4033 0.10 0.500 0 80.7% 42 105 0.425 5.33% 28 2,4,5-T 0.4001 0.10 0.500 0 80.0% 36 105 0.423 5.47% 26 2,4-DB 4.222 1.0 5.00 0 84.4% 44 110 4.41 4.44% 27 Dinoseb 0.7884 0.20 1.00 0 78.8% 29 102 0.777 1.46% 35 2,3-D 4.04 0.10 5.00 0 80.9% 35 119 4.12 1.72% 20 Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank 1-Analyte detected below quantitation limits R-RPD outside accepted recovery limits