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° SEATTLE,WA 11720 NORTH CREEK PKWY N,SUITE 400 <br /> TestAmerica <br /> t3oTNEu,WA 98011-8244 <br /> PH:(425)420.9200 FAX:(425)420.9210 <br /> THE LEADER IN ENVIRONMENTAL TESTING <br /> Huff&Huff Project Name: Stockton Facility <br /> 915 Harger Road,Suite 330 Project Number: MI-080509 Report Created: <br /> Oak Brook,IL 60523 Project Manager: Maureen Wunderlich 05/27/08 14:40 <br /> Extractable Petroleum Hydrocarbons by WDOE TPH Policy Method - Laboratory Quality Control Results <br /> TestAmerica Seattle <br /> QC Batch: 8E14021 Water Preparation Method: EPA 3520C <br /> Analyte Method Result MDL* MRL Units Dil Source Spike "i (Limits) '/ (Limits) Analyzed Notes <br /> Result Amt REC RPD <br /> Blank (8E14021-BLK3) Extracted: 05/14/0810:13 <br /> CB-CIO Aliphatics WA ND <br /> -- 50.0 upfl Ix 05/27/0811:00 <br /> MTCA-EPH <br /> CIO-C12 Aliphatics ND - 50.0 " <br /> Cl2-C 16 Aliphatics ND - 50.0 " <br /> C16-C21 Aliphatics ND - 50.0 " <br /> C21-04 Aliphatics ND - 50.0 " <br /> CS-C IO Aromatics ND - 50.0 -- -- -- -- -- -- 05/23/0821:38 <br /> CIO-C12 Aromatics ND --- 50.0 " <br /> Cl2-C 16 Aromati cs ND --- 50.0 " <br /> C16-C21 Aromatics ND -- 50.0 " <br /> C21-C34 Aromatics ND -- 50.0 " <br /> Surrogate(s): o4erphenyl Recovery: /01% Limits: 60-140% 05123/082/:38 <br /> I-Chloronetadecane 93.1% 60-140% 05127108//:00 <br /> LCS (8E14021-BS3) Extracted: 05/14/0810:13 <br /> C8-C IO Aliphatics WA 167 - 50.0 119/1 Ix - 300 55.8% (50-150) - -- 05/27/0811:29 <br /> MTCA-EPH <br /> CIO-C12 Aliphatics 78.0 -- 50.0 - 100 78.0Ye (70-130) - <br /> C12-C16 Aliphatics 181 -- 50.0 -- 200 90.6% <br /> C16-C21 Aliphatics 307 - 50.0 - 300 102% <br /> C21-C34 Aliphatics 542 - 50.0 - 600 90.4% <br /> C11-CIO Aromatics 73.6 - 50.0 - 100 73.6% (50-150) - - 05/23/08 22:37 <br /> CIO-Cl2 Aromatics 85.6 - 50.0 - 85.6% (70-130) -- - " <br /> Cl2-C 16 Aromatic 257 - 50.0 -- 300 85.8% <br /> C16-C21 Aromatic 478 - 50.0 - 500 95.6% <br /> C21-C34 Aromatics 742 - 50.0 - 800 92.8% <br /> Surrogate(s): a-Terphenyl Recovery: 101% Limits. 60./40% 05/13/0822:37 <br /> l-Chlomoctadecane 94.4% 60-140% 05127,1O8 1I:2Y <br /> LCS Dup (8E14021-BSD3) Extracted: 05/14/0810:13 <br /> 0-CIOAliphatics WA 159 -- 50.0 u9A Ix - 300 53.1% (50-150) 4.99% (25) 05/27!081158 <br /> MICA-EPH <br /> C10-Cl2 Aliphatics 88.3 -- 50.0 -- 100 98.3% (70-130) 12.3% " " <br /> Cl2-C 16 Aliphatics 199 -- 50.0 - 200 99.3% 9.25% " <br /> C16-C21 Aliphatics 327 --- 50.0 -- 300 1091/6 6.23% " <br /> C21-C34 Aliphatics 588 -- 50.0 - 600 97.9% 8.01% " <br /> C8-CIO Aromatics 74.9 -- 50.0 -- 100 74.9% (50-150) 1.75% 05/23/08 23:35 <br /> CIO-C 12 Aromatics 88.8 --- 50.0 -- 88.8% (70-130) 3.67% " <br /> C12-C16 Aromatics 280 --- 50.0 •- 300 93.4% 8.44% " <br /> C16-C21 Aromatics 511 --- 50.0 - 500 102% 6.78% " <br /> C21-C34 Aromatics 799 --- 50.0 - 800 99.9% 7.44% " <br /> TestAmerica Seattle 7be results in this report apply to the samples analysed in accordance with the chain <br /> of custody document.This analytical repos shall not be reproduced except in fid/. <br /> without the written approval of the laboratory. <br /> Curtis D.Armstrong,Proiect Manager <br /> wwwtestamericainc. com Page4of6 <br />