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A N A L Y T I C A L <br />ATORIE S <br />LABO- <br />R <br />Maureen Daggett Certificate of Analysis <br />ECM Services Report Issue Date: 03/22/2000 <br />9437 Elm Avenue <br />Orangevale, CA 95662 <br />BSK Submission #: 2000030010 <br />BSK Sample ID #: 27514 <br />Project ID: Project Desc: QBR-Stormw ate r-QBR II <br />Submission Comments: <br />Sample Tvpe: Liquid <br />Sample Description: Storm water -Main Drain Cal ipar Yard <br />Sample Comments: Samplin)4Times 0900-0930. <br />Date Sampled: 02/29/2000 <br />Time Sampled: <br />Date Received: 03;01/2000 <br />Inorganics <br />Prep <br />Analvsis <br />Method <br />Result <br />Units <br />PQL <br />Dilution <br />DLR <br />Date <br />Date <br />Analvte <br />EPA 200.7 <br />ND <br />mg/L <br />0.01 <br />1 <br />0.01 <br />03/02/2000 <br />03/07/2000 <br />Cadmium (Cd) <br />Chemical Oxygen Demand (COD) <br />SM 5220-D <br />40 <br />mg/L <br />5 <br />1 <br />5 <br />03/08/2000 <br />03/08/2000 <br />Conductivity - Specific (EC) <br />SM 2510 B <br />240 <br />µmho/cm <br />I <br />1 <br />1 <br />03/02/2000 <br />03/02/2000 <br />EPA 200.7 <br />ND <br />mg/L <br />0.05 <br />1 <br />0.05 <br />03/02/2000 <br />03/07/2000 <br />Copper (Cu) <br />EPA 200.7 <br />ND <br />mg/L <br />0.05 <br />1 <br />0.05 <br />03/02/2000 <br />03/07/2000 <br />Lead (Pb) <br />EPA 200.8 <br />18 <br />µg/l- <br />10 <br />1 <br />10 <br />03/14/2000 <br />03/16/2000 <br />Nickel (Ni) <br />EPA 9040 <br />6.54 <br />STD <br />- <br />1 <br />N/A <br />03/16/2000 <br />03/16/2000 <br />pH <br />Solids - Total Suspended (TSS) <br />SM 2540-D <br />44 <br />mg/L <br />5 <br />1 <br />5 <br />03/02/2000 <br />03/03/2000 <br />Total Organic Carbon (TOC) <br />SM 5310-C <br />13 <br />mg/L <br />0.2 <br />5 <br />1.0 <br />03/09/2000 <br />03/09/2000 <br />EPA 200.7 <br />ND <br />mg/L <br />0.05 <br />1 <br />0.05 <br />03/02/2000 <br />03/07/2000 <br />Zinc (Zn) <br />m>:/L: milliQramS./liter (ppm) PQL: practical quantitation limit H: analyzed outside of hold time <br />mg/Kg: illig ams!likilogrMilm (pprn) DLR: detection I imi t for reporti ng P: preliminary result <br />PQL x Dilution S: suspect result <br />µg/L: micrograms/liter (ppb) <br />(ppb) ND: none detected at DLR <br />µg/Kg: microgralns/kilogram <br />%Rec: percent recovered (surrogate i) <br />1414 Stanislaus Street Fresno CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935 <br />H <br />